(1S,2S,3S,6R)-6-acetylamino-1,2-O-isopropylidene-3-cyclohexylcyclohex-4-ene-1,2,3-triol

Base Information

Chemical Name:(1S,2S,3S,6R)-6-acetylamino-1,2-O-isopropylidene-3-cyclohexylcyclohex-4-ene-1,2,3-triol
CAS No.:1229922-77-3
Molecular Formula:C₁₇H₂₇NO₄
Molecular Weight:309.406
Hs Code.:

Synonyms:(1S,2S,3S,6R)-6-acetylamino-1,2-O-isopropylidene-3-cyclohexylcyclohex-4-ene-1,2,3-triol

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Chemical Property of (1S,2S,3S,6R)-6-acetylamino-1,2-O-isopropylidene-3-cyclohexylcyclohex-4-ene-1,2,3-triol

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Technology Process of (1S,2S,3S,6R)-6-acetylamino-1,2-O-isopropylidene-3-cyclohexylcyclohex-4-ene-1,2,3-triol

There total 1 articles about (1S,2S,3S,6R)-6-acetylamino-1,2-O-isopropylidene-3-cyclohexylcyclohex-4-ene-1,2,3-triol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 1229922-74-0
3-acetyl-1-cyclohexyl-5,6-O-isopropylidene-2-oxa-3-azabicyclo[2.2.2]oct-7-ene-5,6-diol

: 1229922-77-3
(1S,2S,3S,6R)-6-acetylamino-1,2-O-isopropylidene-3-cyclohexylcyclohex-4-ene-1,2,3-triol

Guidance literature:: With water; molybdenum hexacarbonyl; In acetonitrile; Reflux;
DOI:10.1016/j.tet.2010.03.059

Reference yield: 68.0%

: 1229922-77-3
(1S,2S,3S,6R)-6-acetylamino-1,2-O-isopropylidene-3-cyclohexylcyclohex-4-ene-1,2,3-triol

: 1229922-79-5
(3aR,5aR,8aR,8bS)-2,2,7-trimethyl-4-cyclohexyl-3a,5a,8a,8b-tetrahydro[1,3]dioxolo[4,5-e][1,3]benzoxazole

Guidance literature:: With triethylamine; Methanesulfonic anhydride; In 1,2-dichloro-ethane; at 4 - 15 ℃; stereoselective reaction;
DOI:10.1016/j.tet.2010.03.059

Reference yield: 58.0%

: 1229922-77-3
(1S,2S,3S,6R)-6-acetylamino-1,2-O-isopropylidene-3-cyclohexylcyclohex-4-ene-1,2,3-triol

: 1229922-81-9
N-((3aS,4R,5R,7aR)-7-cyclohexyl-5-hydroxy-2,2-dimethyl-3a,4,5,7a-tetrahydrobenzo[d][1,3]dioxol-4-yl)acetamide

Guidance literature:: (1S,2S,3S,6R)-6-acetylamino-1,2-O-isopropylidene-3-cyclohexylcyclohex-4-ene-1,2,3-triol; With methanesulfonyl chloride; triethylamine; In 1,2-dichloro-ethane; at 4 - 60 ℃;

With ethanol; sodium hydroxide; at 90 ℃; for 17h; pH=8 - 10;
DOI:10.1016/j.tet.2010.03.059