N-((3aS,4R,5R,7aR)-7-cyclohexyl-5-hydroxy-2,2-dimethyl-3a,4,5,7a-tetrahydrobenzo[d][1,3]dioxol-4-yl)acetamide

Base Information

• Chemical Name: N-((3aS,4R,5R,7aR)-7-cyclohexyl-5-hydroxy-2,2-dimethyl-3a,4,5,7a-tetrahydrobenzo[d][1,3]dioxol-4-yl)acetamide
• CAS No.: 1229922-81-9
• Molecular Formula: C₁₇H₂₇NO₄
• Molecular Weight: 309.406

Synonyms:N-((3aS,4R,5R,7aR)-7-cyclohexyl-5-hydroxy-2,2-dimethyl-3a,4,5,7a-tetrahydrobenzo[d][1,3]dioxol-4-yl)acetamide

Chemical Property of N-((3aS,4R,5R,7aR)-7-cyclohexyl-5-hydroxy-2,2-dimethyl-3a,4,5,7a-tetrahydrobenzo[d][1,3]dioxol-4-yl)acetamide

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Technology Process of N-((3aS,4R,5R,7aR)-7-cyclohexyl-5-hydroxy-2,2-dimethyl-3a,4,5,7a-tetrahydrobenzo[d][1,3]dioxol-4-yl)acetamide

There total 1 articles about N-((3aS,4R,5R,7aR)-7-cyclohexyl-5-hydroxy-2,2-dimethyl-3a,4,5,7a-tetrahydrobenzo[d][1,3]dioxol-4-yl)acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

(1S,2S,3S,6R)-6-acetylamino-1,2-O-isopropylidene-3-cyclohexylcyclohex-4-ene-1,2,3-triol (1229922-77-3) → N-((3aS,4R,5R,7aR)-7-cyclohexyl-5-hydroxy-2,2-dimethyl-3a,4,5,7a-tetrahydrobenzo[d][1,3]dioxol-4-yl)acetamide (1229922-81-9)

Guidance literature:

(1S,2S,3S,6R)-6-acetylamino-1,2-O-isopropylidene-3-cyclohexylcyclohex-4-ene-1,2,3-triol; With methanesulfonyl chloride; triethylamine; In 1,2-dichloro-ethane; at 4 - 60 ℃;

With ethanol; sodium hydroxide; at 90 ℃; for 17h; pH=8 - 10;

DOI:10.1016/j.tet.2010.03.059

Reference yield:

N-((3aS,4R,5R,7aR)-7-cyclohexyl-5-hydroxy-2,2-dimethyl-3a,4,5,7a-tetrahydrobenzo[d][1,3]dioxol-4-yl)acetamide (1229922-81-9) + methanesulfonyl chloride (124-63-0) → C18H29NO6S (1229922-83-1)

Guidance literature:

With triethylamine; In 1,2-dichloro-ethane; at -78 - 0 ℃;

DOI:10.1016/j.tet.2010.03.059

upstream raw materials:

(1S,2S,3S,6R)-6-acetylamino-1,2-O-isopropylidene-3-cyclohexylcyclohex-4-ene-1,2,3-triol

Downstream raw materials:

C₁₈H₂₉NO₆S

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