N-((bis(2,4,6-trimethylbenzoyl)phosphino)methyl)-N,N,N-trimethylammonium triflate

Base Information

Chemical Name:N-((bis(2,4,6-trimethylbenzoyl)phosphino)methyl)-N,N,N-trimethylammonium triflate
CAS No.:1591653-24-5
Molecular Formula:CF₃O₃S*C₂₄H₃₃NO₂P
Molecular Weight:547.576
Hs Code.:

Synonyms:N-((bis(2,4,6-trimethylbenzoyl)phosphino)methyl)-N,N,N-trimethylammonium triflate

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Chemical Property of N-((bis(2,4,6-trimethylbenzoyl)phosphino)methyl)-N,N,N-trimethylammonium triflate

Chemical Property:

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Technology Process of N-((bis(2,4,6-trimethylbenzoyl)phosphino)methyl)-N,N,N-trimethylammonium triflate

There total 3 articles about N-((bis(2,4,6-trimethylbenzoyl)phosphino)methyl)-N,N,N-trimethylammonium triflate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1591653-20-1
N-((bis(2,4,6-trimethylbenzoyl)phosphino)methyl)-N,N-dimethylamine

: 333-27-7
methyl trifluoromethanesulfonate

: 1591653-24-5
N-((bis(2,4,6-trimethylbenzoyl)phosphino)methyl)-N,N,N-trimethylammonium triflate

Guidance literature:: In tetrahydrofuran; at 20 ℃; for 2h;

Reference yield:

: 1253120-30-7
sodium bis(2,4,6-trimethylbenzoyl)phosphanide

: 1591653-24-5
N-((bis(2,4,6-trimethylbenzoyl)phosphino)methyl)-N,N,N-trimethylammonium triflate

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / toluene; tetrahydrofuran / 12 h / 20 °C / Schlenk technique; Inert atmosphere

2: tetrahydrofuran / 2 h / 20 °C

With triethylamine; In tetrahydrofuran; toluene;

Reference yield:

: 938-18-1
mesitylene-2-carboxylic acid chloride

: 1591653-24-5
N-((bis(2,4,6-trimethylbenzoyl)phosphino)methyl)-N,N,N-trimethylammonium triflate

Guidance literature:: Multi-step reaction with 3 steps

1: sodium; phosphorus; ammonia; tert-butyl alcohol / 1,2-dimethoxyethane / 1 h / 20 °C / Schlenk technique; Inert atmosphere

2: triethylamine / toluene; tetrahydrofuran / 12 h / 20 °C / Schlenk technique; Inert atmosphere

3: tetrahydrofuran / 2 h / 20 °C

With phosphorus; ammonia; sodium; triethylamine; tert-butyl alcohol; In tetrahydrofuran; 1,2-dimethoxyethane; toluene;