N²-(3,5-dichlorophenyl)-9-<<1,3-bis(benzyloxy)-2-propoxy>methyl>guanine

Base Information

Chemical Name:N²-(3,5-dichlorophenyl)-9-<<1,3-bis(benzyloxy)-2-propoxy>methyl>guanine
CAS No.:163020-81-3
Molecular Formula:C₂₉H₂₇Cl₂N₅O₄
Molecular Weight:580.47
Hs Code.:

N<sup>2</sup>-(3,5-dichlorophenyl)-9-<<1,3-bis(benzyloxy)-2-propoxy>methyl>guanine

Synonyms:N²-(3,5-dichlorophenyl)-9-<<1,3-bis(benzyloxy)-2-propoxy>methyl>guanine

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Chemical Property of N²-(3,5-dichlorophenyl)-9-<<1,3-bis(benzyloxy)-2-propoxy>methyl>guanine

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Technology Process of N²-(3,5-dichlorophenyl)-9-<<1,3-bis(benzyloxy)-2-propoxy>methyl>guanine

There total 4 articles about N²-(3,5-dichlorophenyl)-9-<<1,3-bis(benzyloxy)-2-propoxy>methyl>guanine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

: 163020-64-2
2-(3,5-dichloroanilino)-6-chloro-9-<<1,3-bis(benzyloxy)-2-propoxy>methyl>purine

: 163020-81-3
N²-(3,5-dichlorophenyl)-9-<<1,3-bis(benzyloxy)-2-propoxy>methyl>guanine

Guidance literature:: With sodium methylate; 2-hydroxyethanethiol; In methanol; for 30h; Heating;
DOI:10.1021/jm00010a026

Reference yield:

: 74564-16-2
1,3-dibenzyloxy-2-(chloromethoxy)propane

: 163020-81-3
N²-(3,5-dichlorophenyl)-9-<<1,3-bis(benzyloxy)-2-propoxy>methyl>guanine

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) NaH / 1.) DMF, RT, 45 min, 2.) DMF, RT, 1.5 h

2: 52 percent / 2-mercaptoethanol, sodium methoxide / methanol / 30 h / Heating

With sodium methylate; sodium hydride; 2-hydroxyethanethiol; In methanol;
DOI:10.1021/jm00010a026

Reference yield:

: 163020-52-8
2-(3,5-dichloroanilino)-6-chloropurine

: 163020-81-3
N²-(3,5-dichlorophenyl)-9-<<1,3-bis(benzyloxy)-2-propoxy>methyl>guanine

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) NaH / 1.) DMF, RT, 45 min, 2.) DMF, RT, 1.5 h

2: 52 percent / 2-mercaptoethanol, sodium methoxide / methanol / 30 h / Heating

With sodium methylate; sodium hydride; 2-hydroxyethanethiol; In methanol;
DOI:10.1021/jm00010a026