(1R,4S,5R,6R)-4,5,6-tris(benzyloxy)-1-(benzyloxymethyl)cyclohex-2-en-1-ol

Base Information

Chemical Name:(1R,4S,5R,6R)-4,5,6-tris(benzyloxy)-1-(benzyloxymethyl)cyclohex-2-en-1-ol
CAS No.:1161147-20-1
Molecular Formula:C₃₅H₃₆O₅
Molecular Weight:536.668
Hs Code.:

Synonyms:(1R,4S,5R,6R)-4,5,6-tris(benzyloxy)-1-(benzyloxymethyl)cyclohex-2-en-1-ol

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Chemical Property of (1R,4S,5R,6R)-4,5,6-tris(benzyloxy)-1-(benzyloxymethyl)cyclohex-2-en-1-ol

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Technology Process of (1R,4S,5R,6R)-4,5,6-tris(benzyloxy)-1-(benzyloxymethyl)cyclohex-2-en-1-ol

There total 1 articles about (1R,4S,5R,6R)-4,5,6-tris(benzyloxy)-1-(benzyloxymethyl)cyclohex-2-en-1-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 1161147-17-6
(3R,4R,5R,6S)-4,5,6-tris(benzyloxy)-3-(benzyloxymethyl)octa-1,7-dien-3-ol

: 1161147-20-1,1219194-46-3
(1R,4S,5R,6R)-4,5,6-tris(benzyloxy)-1-(benzyloxymethyl)cyclohex-2-en-1-ol

Guidance literature:: With tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; In chloroform; at 20 ℃; for 48h; Inert atmosphere;
DOI:10.1021/ol9008987

Reference yield: 86.0%

: 1161147-20-1,1219194-46-3
(1R,4S,5R,6R)-4,5,6-tris(benzyloxy)-1-(benzyloxymethyl)cyclohex-2-en-1-ol

: 108-24-7
acetic anhydride

: 1161745-98-7
C₁₅H₂₀O₉

Guidance literature:: (1R,4S,5R,6R)-4,5,6-tris(benzyloxy)-1-(benzyloxymethyl)cyclohex-2-en-1-ol; With boron trichloride; In dichloromethane; at -78 - 0 ℃; Inert atmosphere;

acetic anhydride; With pyridine; at 20 ℃; for 15h;
DOI:10.1021/ol9008987

Reference yield: 71.0%

: 1161147-20-1,1219194-46-3
(1R,4S,5R,6R)-4,5,6-tris(benzyloxy)-1-(benzyloxymethyl)cyclohex-2-en-1-ol

: 75-36-5
acetyl chloride

: 1161147-22-3
(1R,4S,5R,6R)-4,5,6-tris(benzyloxy)-1-(benzyloxymethyl)cyclohex-2-en-1-yl acetate

Guidance literature:: (1R,4S,5R,6R)-4,5,6-tris(benzyloxy)-1-(benzyloxymethyl)cyclohex-2-en-1-ol; With lithium hexamethyldisilazane; In tetrahydrofuran; at 0 ℃; for 0.5h; Inert atmosphere;

acetyl chloride; In tetrahydrofuran; at 20 ℃; for 24h; Inert atmosphere;
DOI:10.1021/ol9008987