Technology Process of C60H34O
There total 3 articles about C60H34O which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
sodium t-butanolate;
tri-tert-butyl phosphine; palladium diacetate;
In
toluene;
at 100 ℃;
for 24h;
Inert atmosphere;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: lithium hydroxide monohydrate / dichloromethane / 4 h / 25 °C
2: 2,3-dicyano-5,6-dichloro-p-benzoquinone / chlorobenzene / 2 h / Reflux; Inert atmosphere
3: sodium t-butanolate / palladium diacetate; tri-tert-butyl phosphine / toluene / 24 h / 100 °C / Inert atmosphere
With
lithium hydroxide monohydrate; 2,3-dicyano-5,6-dichloro-p-benzoquinone; sodium t-butanolate;
tri-tert-butyl phosphine; palladium diacetate;
In
dichloromethane; chlorobenzene; toluene;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 2,3-dicyano-5,6-dichloro-p-benzoquinone / chlorobenzene / 2 h / Reflux; Inert atmosphere
2: sodium t-butanolate / palladium diacetate; tri-tert-butyl phosphine / toluene / 24 h / 100 °C / Inert atmosphere
With
2,3-dicyano-5,6-dichloro-p-benzoquinone; sodium t-butanolate;
tri-tert-butyl phosphine; palladium diacetate;
In
chlorobenzene; toluene;