2-(1′,3′-bis(pentafluorophenyl)-1,3,2-benzodiazaborolyl)-5-(1″,3″-diethyl-1″,3″,2″-benzodiazaborolyl)-thiophene

Base Information

Chemical Name:2-(1′,3′-bis(pentafluorophenyl)-1,3,2-benzodiazaborolyl)-5-(1″,3″-diethyl-1″,3″,2″-benzodiazaborolyl)-thiophene
CAS No.:1558041-60-3
Molecular Formula:C₃₂H₂₀B₂F₁₀N₄S
Molecular Weight:704.21
Hs Code.:

Synonyms:2-(1′,3′-bis(pentafluorophenyl)-1,3,2-benzodiazaborolyl)-5-(1″,3″-diethyl-1″,3″,2″-benzodiazaborolyl)-thiophene

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Chemical Property of 2-(1′,3′-bis(pentafluorophenyl)-1,3,2-benzodiazaborolyl)-5-(1″,3″-diethyl-1″,3″,2″-benzodiazaborolyl)-thiophene

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Technology Process of 2-(1′,3′-bis(pentafluorophenyl)-1,3,2-benzodiazaborolyl)-5-(1″,3″-diethyl-1″,3″,2″-benzodiazaborolyl)-thiophene

There total 3 articles about 2-(1′,3′-bis(pentafluorophenyl)-1,3,2-benzodiazaborolyl)-5-(1″,3″-diethyl-1″,3″,2″-benzodiazaborolyl)-thiophene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 46.0%

: 214604-82-7
N,N′-bis(pentafluorophenyl)phenylenediamine

: 1558041-78-3
C₃₂H₃₁B₂Br₂N₂PS

: 1558041-60-3
2-(1′,3′-bis(pentafluorophenyl)-1,3,2-benzodiazaborolyl)-5-(1″,3″-diethyl-1″,3″,2″-benzodiazaborolyl)-thiophene

Guidance literature:: With 2,2,6,6-tetramethyl-piperidine; In toluene; at 100 ℃; for 16h; Inert atmosphere; Schlenk technique;
DOI:10.1039/c3dt52836g

Reference yield:

: 1,3-diethyl-2-(5′-trimethylsilyl-thien-2′-yl)-1,3,2-benzodiazaborole

: 1558041-60-3
2-(1′,3′-bis(pentafluorophenyl)-1,3,2-benzodiazaborolyl)-5-(1″,3″-diethyl-1″,3″,2″-benzodiazaborolyl)-thiophene

Guidance literature:: Multi-step reaction with 3 steps

1: dichloromethane / 1 h / 20 °C / Inert atmosphere; Schlenk technique

2: dichloromethane / 2 h / Inert atmosphere; Schlenk technique

3: 2,2,6,6-tetramethyl-piperidine / toluene / 16 h / 100 °C / Inert atmosphere; Schlenk technique

With 2,2,6,6-tetramethyl-piperidine; In dichloromethane; toluene;
DOI:10.1039/c3dt52836g

Reference yield:

: 1558041-77-2
C₁₄H₁₆B₂Br₂N₂S

: 1558041-60-3
2-(1′,3′-bis(pentafluorophenyl)-1,3,2-benzodiazaborolyl)-5-(1″,3″-diethyl-1″,3″,2″-benzodiazaborolyl)-thiophene

Guidance literature:: Multi-step reaction with 2 steps

1: dichloromethane / 2 h / Inert atmosphere; Schlenk technique

2: 2,2,6,6-tetramethyl-piperidine / toluene / 16 h / 100 °C / Inert atmosphere; Schlenk technique

With 2,2,6,6-tetramethyl-piperidine; In dichloromethane; toluene;
DOI:10.1039/c3dt52836g