(R)-ethyl 6-oxo-4-phenyl-1-tosyl-1,2,3,6-tetrahydropyridine-2-carboxylate

Base Information

Chemical Name:(R)-ethyl 6-oxo-4-phenyl-1-tosyl-1,2,3,6-tetrahydropyridine-2-carboxylate
CAS No.:1581699-94-6
Molecular Formula:C₂₁H₂₁NO₅S
Molecular Weight:399.467
Hs Code.:

Synonyms:(R)-ethyl 6-oxo-4-phenyl-1-tosyl-1,2,3,6-tetrahydropyridine-2-carboxylate

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Chemical Property of (R)-ethyl 6-oxo-4-phenyl-1-tosyl-1,2,3,6-tetrahydropyridine-2-carboxylate

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Technology Process of (R)-ethyl 6-oxo-4-phenyl-1-tosyl-1,2,3,6-tetrahydropyridine-2-carboxylate

There total 6 articles about (R)-ethyl 6-oxo-4-phenyl-1-tosyl-1,2,3,6-tetrahydropyridine-2-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 36935-06-5
2-(p-Tolylsulfonylamino)acrylic acid ethyl ester

: 104-55-2
3-phenyl-propenal

: 1581699-94-6
(R)-ethyl 6-oxo-4-phenyl-1-tosyl-1,2,3,6-tetrahydropyridine-2-carboxylate

Guidance literature:: With 1,4-diaza-bicyclo[2.2.2]octane; (5aR,10bS)-2-phenyl-4,5a,6,10b-tetrahydroindeno[2,1-b][1,2,4]triazolo[4,3-d][1,4]-oxazin-2-ium tetrafluoroborate; 3,5,3',5'-tetra-tert-butyl-4,4'-diphenoquinone; In tetrahydrofuran; at 20 ℃;
DOI:10.1039/c7cc02753b

Reference yield: 65.0%

: C₂₁H₂₁NO₅S

: 1581699-94-6
(R)-ethyl 6-oxo-4-phenyl-1-tosyl-1,2,3,6-tetrahydropyridine-2-carboxylate

Guidance literature:: With 1,4-diaza-bicyclo[2.2.2]octane; In tetrahydrofuran; at 20 ℃; for 12h; Schlenk technique; Sealed tube; Inert atmosphere;
DOI:10.1039/c7cc02753b

Reference yield: 48.0%

: 68204-17-1
3-phenylbut-2-enoyl chloride

: 83670-53-5
ethyl (N-tosylimino)acetate

: 1581699-94-6
(R)-ethyl 6-oxo-4-phenyl-1-tosyl-1,2,3,6-tetrahydropyridine-2-carboxylate

Guidance literature:: With O-(trimethylsilyl)quinine; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; diethyl ether; at -40 ℃; enantioselective reaction; Schlenk technique; Molecular sieve; Inert atmosphere;
DOI:10.1039/c4ob00114a