C₃₂H₃₉BN₂O₁₀

Base Information

Chemical Name:C₃₂H₃₉BN₂O₁₀
CAS No.:1425052-04-5
Molecular Formula:C₃₂H₃₉BN₂O₁₀
Molecular Weight:622.48
Hs Code.:

C<sub>32</sub>H<sub>39</sub>BN<sub>2</sub>O<sub>10</sub>

Synonyms:C₃₂H₃₉BN₂O₁₀

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Chemical Property of C₃₂H₃₉BN₂O₁₀

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Technology Process of C₃₂H₃₉BN₂O₁₀

There total 9 articles about C₃₂H₃₉BN₂O₁₀ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: 1425052-03-4
C₃₈H₅₃BN₂O₁₀Si

: 1425052-04-5
C₃₂H₃₉BN₂O₁₀

Guidance literature:: With toluene-4-sulfonic acid; In tetrahydrofuran; water; at 23 ℃; for 8h;
DOI:10.1021/jo400105m

Reference yield:

: 136507-15-8
4-nitro-2-methoxybenzaldehyde

: 1425052-04-5
C₃₂H₃₉BN₂O₁₀

Guidance literature:: Multi-step reaction with 6 steps

1: sodium tetrahydroborate / dichloromethane; methanol / 0.25 h / 0 °C / Inert atmosphere

2: dmap; 1H-imidazole / dichloromethane / 1 h / 23 °C / Inert atmosphere

3: palladium 10% on activated carbon; hydrogen / tetrahydrofuran / 1.5 h / 23 °C / Inert atmosphere

4: sodium hydrogencarbonate / tetrahydrofuran; water / 0.25 h / 23 °C

5: dibutyltin(II) dilaurate / toluene / 2 h / 110 °C / Inert atmosphere

6: toluene-4-sulfonic acid / tetrahydrofuran; water / 8 h / 23 °C

With 1H-imidazole; dmap; dibutyltin(II) dilaurate; sodium tetrahydroborate; palladium 10% on activated carbon; hydrogen; sodium hydrogencarbonate; toluene-4-sulfonic acid; In tetrahydrofuran; methanol; dichloromethane; water; toluene;
DOI:10.1021/jo400105m

Reference yield:

: 136507-14-7
(2-methoxy-4-nitrophenyl)methanol

: 1425052-04-5
C₃₂H₃₉BN₂O₁₀

Guidance literature:: Multi-step reaction with 5 steps

1: dmap; 1H-imidazole / dichloromethane / 1 h / 23 °C / Inert atmosphere

2: palladium 10% on activated carbon; hydrogen / tetrahydrofuran / 1.5 h / 23 °C / Inert atmosphere

3: sodium hydrogencarbonate / tetrahydrofuran; water / 0.25 h / 23 °C

4: dibutyltin(II) dilaurate / toluene / 2 h / 110 °C / Inert atmosphere

5: toluene-4-sulfonic acid / tetrahydrofuran; water / 8 h / 23 °C

With 1H-imidazole; dmap; dibutyltin(II) dilaurate; palladium 10% on activated carbon; hydrogen; sodium hydrogencarbonate; toluene-4-sulfonic acid; In tetrahydrofuran; dichloromethane; water; toluene;
DOI:10.1021/jo400105m