(S)-1-(1-(benzyloxy)-3-(p-nitrophenylsulfonamido)propan-2-yl)naphthalen-2-yl 4-nitrobenzenesulfonate

Base Information

Chemical Name:(S)-1-(1-(benzyloxy)-3-(p-nitrophenylsulfonamido)propan-2-yl)naphthalen-2-yl 4-nitrobenzenesulfonate
CAS No.:1350980-17-4
Molecular Formula:C₃₂H₂₇N₃O₁₀S₂
Molecular Weight:677.712
Hs Code.:

Synonyms:(S)-1-(1-(benzyloxy)-3-(p-nitrophenylsulfonamido)propan-2-yl)naphthalen-2-yl 4-nitrobenzenesulfonate

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Chemical Property of (S)-1-(1-(benzyloxy)-3-(p-nitrophenylsulfonamido)propan-2-yl)naphthalen-2-yl 4-nitrobenzenesulfonate

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Technology Process of (S)-1-(1-(benzyloxy)-3-(p-nitrophenylsulfonamido)propan-2-yl)naphthalen-2-yl 4-nitrobenzenesulfonate

There total 6 articles about (S)-1-(1-(benzyloxy)-3-(p-nitrophenylsulfonamido)propan-2-yl)naphthalen-2-yl 4-nitrobenzenesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

: 1350980-15-2
(S)-1-(1-amino-3-(benzyloxy)propan-2-yl)naphthalen-2-ol

: 98-74-8
4-Nitrobenzenesulfonyl chloride

: 1350980-17-4
(S)-1-(1-(benzyloxy)-3-(p-nitrophenylsulfonamido)propan-2-yl)naphthalen-2-yl 4-nitrobenzenesulfonate

Guidance literature:: With pyridine; at 40 ℃; for 18h;
DOI:10.1016/j.tetlet.2011.10.105

Reference yield:

: 100-44-7
benzyl chloride

: 1350980-17-4
(S)-1-(1-(benzyloxy)-3-(p-nitrophenylsulfonamido)propan-2-yl)naphthalen-2-yl 4-nitrobenzenesulfonate

Guidance literature:: Multi-step reaction with 5 steps

1.1: potassium hydroxide

1.2: 10 - 60 °C

2.1: ammonium cerium (IV) nitrate; sodium nitrite / acetonitrile / 0 - 20 °C

3.1: C₂₈H₂₈F₆N₄S / toluene / 96 h / -50 °C / Molecular sieve

4.1: ammonium chloride; zinc / ethanol; water / 72 h / 20 °C

5.1: pyridine / 18 h / 40 °C

With pyridine; ammonium cerium (IV) nitrate; C₂₈H₂₈F₆N₄S; ammonium chloride; potassium hydroxide; zinc; sodium nitrite; In ethanol; water; toluene; acetonitrile; 3.1: Friedel Crafts alkylation;
DOI:10.1016/j.tetlet.2011.10.105

Reference yield:

: 1350980-13-0
(S)-1-(1-(benzyloxy)-3-nitropropan-2-yl)naphthalen-2-ol

: 1350980-17-4
(S)-1-(1-(benzyloxy)-3-(p-nitrophenylsulfonamido)propan-2-yl)naphthalen-2-yl 4-nitrobenzenesulfonate

Guidance literature:: Multi-step reaction with 2 steps

1: ammonium chloride; zinc / ethanol; water / 72 h / 20 °C

2: pyridine / 18 h / 40 °C

With pyridine; ammonium chloride; zinc; In ethanol; water;
DOI:10.1016/j.tetlet.2011.10.105