(+)-2-<(2-azidoethoxy)methyl>-4-(2-chlorophenyl)-5-(methoxycarbonyl)-3-<(2(S)-methoxy-2-phenethoxy)carbonyl>-6-methyl-1,4-dihydropyridine

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Chemical Name:(+)-2-<(2-azidoethoxy)methyl>-4-(2-chlorophenyl)-5-(methoxycarbonyl)-3-<(2(S)-methoxy-2-phenethoxy)carbonyl>-6-methyl-1,4-dihydropyridine
CAS No.:103094-34-4
Molecular Formula:C₂₇H₂₉ClN₄O₆
Molecular Weight:541.003
Hs Code.:
Mol file:103094-34-4.mol

Synonyms:(+)-2-<(2-azidoethoxy)methyl>-4-(2-chlorophenyl)-5-(methoxycarbonyl)-3-<(2(S)-methoxy-2-phenethoxy)carbonyl>-6-methyl-1,4-dihydropyridine

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Chemical Property of (+)-2-<(2-azidoethoxy)methyl>-4-(2-chlorophenyl)-5-(methoxycarbonyl)-3-<(2(S)-methoxy-2-phenethoxy)carbonyl>-6-methyl-1,4-dihydropyridine Edit

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Technology Process of (+)-2-<(2-azidoethoxy)methyl>-4-(2-chlorophenyl)-5-(methoxycarbonyl)-3-<(2(S)-methoxy-2-phenethoxy)carbonyl>-6-methyl-1,4-dihydropyridine

There total 4 articles about (+)-2-<(2-azidoethoxy)methyl>-4-(2-chlorophenyl)-5-(methoxycarbonyl)-3-<(2(S)-methoxy-2-phenethoxy)carbonyl>-6-methyl-1,4-dihydropyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 103069-47-2
2-cyanoethyl 4-(2-azidoethoxy)-3-oxobutanoate

: 103094-34-4
(+)-2-<(2-azidoethoxy)methyl>-4-(2-chlorophenyl)-5-(methoxycarbonyl)-3-<(2(S)-methoxy-2-phenethoxy)carbonyl>-6-methyl-1,4-dihydropyridine

Guidance literature:: Multi-step reaction with 3 steps

1: 41 percent / ethanol / 2 h / Heating

2: 74 percent / aq. NaOH / bis-(2-methoxy-ethyl) ether / 2 h / Ambient temperature

3: 1.) carbonyldiimidazole / 1.) CH₂Cl₂, reflux, 2.) THF, RT, 1 h

With sodium hydroxide; 1,1'-carbonyldiimidazole; In ethanol; diethylene glycol dimethyl ether;
DOI:10.1021/jm00159a022

Reference yield:

: 103069-48-3
2-<(2-azidoethoxy)methyl>-4-(2-chlorophenyl)-3-(2-cyanoethoxycarbonyl)-5-methoxycarbonyl-6-methyl-1,4-dihydropyridine

: 103094-34-4
(+)-2-<(2-azidoethoxy)methyl>-4-(2-chlorophenyl)-5-(methoxycarbonyl)-3-<(2(S)-methoxy-2-phenethoxy)carbonyl>-6-methyl-1,4-dihydropyridine

Guidance literature:: Multi-step reaction with 2 steps

1: 74 percent / aq. NaOH / bis-(2-methoxy-ethyl) ether / 2 h / Ambient temperature

2: 1.) carbonyldiimidazole / 1.) CH₂Cl₂, reflux, 2.) THF, RT, 1 h

With sodium hydroxide; 1,1'-carbonyldiimidazole; In diethylene glycol dimethyl ether;
DOI:10.1021/jm00159a022