2,6-Dichloro-benzoic acid (S)-3-benzyloxycarbonylamino-4-tert-butoxycarbonyl-2-oxo-butyl ester

Base Information

Chemical Name:2,6-Dichloro-benzoic acid (S)-3-benzyloxycarbonylamino-4-tert-butoxycarbonyl-2-oxo-butyl ester
CAS No.:153088-77-8
Molecular Formula:C₂₄H₂₅Cl₂NO₇
Molecular Weight:510.371
Hs Code.:

Synonyms:2,6-Dichloro-benzoic acid (S)-3-benzyloxycarbonylamino-4-tert-butoxycarbonyl-2-oxo-butyl ester

Suppliers and Price of 2,6-Dichloro-benzoic acid (S)-3-benzyloxycarbonylamino-4-tert-butoxycarbonyl-2-oxo-butyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 2,6-Dichloro-benzoic acid (S)-3-benzyloxycarbonylamino-4-tert-butoxycarbonyl-2-oxo-butyl ester

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 2,6-Dichloro-benzoic acid (S)-3-benzyloxycarbonylamino-4-tert-butoxycarbonyl-2-oxo-butyl ester

There total 4 articles about 2,6-Dichloro-benzoic acid (S)-3-benzyloxycarbonylamino-4-tert-butoxycarbonyl-2-oxo-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 153088-76-7
(S)-3-benzyloxycarbonylamino-5-bromo-4-oxo-pentanoic acid tert-butyl ester

: 50-30-6
2,6-dichlorobenzoic acid

: 153088-77-8
2,6-Dichloro-benzoic acid (S)-3-benzyloxycarbonylamino-4-tert-butoxycarbonyl-2-oxo-butyl ester

Guidance literature:: With potassium fluoride; In N,N-dimethyl-formamide; at 25 ℃; for 12h; Yield given;

Reference yield:

: 5545-52-8
Z-D(tBu)-OH

: 153088-77-8
2,6-Dichloro-benzoic acid (S)-3-benzyloxycarbonylamino-4-tert-butoxycarbonyl-2-oxo-butyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: N-methylmorpholine / tetrahydrofuran / -15 °C

2: diethyl ether / -15 - 25 °C

3: HBr / acetic acid / 0 °C

4: KF / dimethylformamide / 12 h / 25 °C

With 4-methyl-morpholine; potassium fluoride; hydrogen bromide; In tetrahydrofuran; diethyl ether; acetic acid; N,N-dimethyl-formamide;

Reference yield:

: (S)-3-Benzyloxycarbonylamino-4-ethoxycarbonyloxy-4-oxo-butyric acid tert-butyl ester

: 153088-77-8
2,6-Dichloro-benzoic acid (S)-3-benzyloxycarbonylamino-4-tert-butoxycarbonyl-2-oxo-butyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: diethyl ether / -15 - 25 °C

2: HBr / acetic acid / 0 °C

3: KF / dimethylformamide / 12 h / 25 °C

With potassium fluoride; hydrogen bromide; In diethyl ether; acetic acid; N,N-dimethyl-formamide;