C₂₆H₃₇N₃O₇

Base Information

Chemical Name:C₂₆H₃₇N₃O₇
CAS No.:1333408-24-4
Molecular Formula:C₂₆H₃₇N₃O₇
Molecular Weight:503.596
Hs Code.:

C<sub>26</sub>H<sub>37</sub>N<sub>3</sub>O<sub>7</sub>

Synonyms:C₂₆H₃₇N₃O₇

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Chemical Property of C₂₆H₃₇N₃O₇

Chemical Property:

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Technology Process of C₂₆H₃₇N₃O₇

There total 8 articles about C₂₆H₃₇N₃O₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 874162-99-9
(2S,4S)-4-(((benzyloxy)carbonyl)amino)-1-(tert-butoxycarbonyl)pyrrolidine-2-carboxylic acid

: 1333408-23-3
C₈H₁₅NO₂

: 1333408-24-4
C₂₆H₃₇N₃O₇

Guidance literature:: (2S,4S)-4-(((benzyloxy)carbonyl)amino)-1-(tert-butoxycarbonyl)pyrrolidine-2-carboxylic acid; With benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; In dichloromethane; for 0.0833333h; Inert atmosphere;

C₈H₁₅NO₂; In dichloromethane; at 20 ℃; for 2h; Inert atmosphere;
DOI:10.1007/s00726-011-0912-4

Reference yield:

: 80-57-9,1196-01-6
(-)-Verbenone

: 1333408-24-4
C₂₆H₃₇N₃O₇

Guidance literature:: Multi-step reaction with 8 steps

1.1: sodium periodate; ruthenium trichloride / dichloromethane; water; acetonitrile / 20 °C

2.1: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / tetrahydrofuran / 0 °C

3.1: sodium hypobromide / 1,4-dioxane; water

4.3: Reflux

5.1: triethylsilane; trifluoroacetic acid / dichloromethane

6.1: caesium carbonate / N,N-dimethyl-formamide

7.1: palladium 10% on activated carbon; ammonium formate / methanol / Reflux

8.1: benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / dichloromethane / 0.08 h / Inert atmosphere

8.2: 2 h / 20 °C / Inert atmosphere

With triethylsilane; dmap; ruthenium trichloride; sodium periodate; sodium hypobromide; palladium 10% on activated carbon; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; ammonium formate; caesium carbonate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; In tetrahydrofuran; 1,4-dioxane; methanol; dichloromethane; water; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1007/s00726-011-0912-4

Reference yield:

: 1017279-80-9
benzyl (1R,3S)-3-tert-butoxycarbonyl-2,2-dimethylcyclobutyl-1-carbamate

: 1333408-24-4
C₂₆H₃₇N₃O₇

Guidance literature:: Multi-step reaction with 4 steps

1.1: triethylsilane; trifluoroacetic acid / dichloromethane

2.1: caesium carbonate / N,N-dimethyl-formamide

3.1: palladium 10% on activated carbon; ammonium formate / methanol / Reflux

4.1: benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / dichloromethane / 0.08 h / Inert atmosphere

4.2: 2 h / 20 °C / Inert atmosphere

With triethylsilane; palladium 10% on activated carbon; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; ammonium formate; caesium carbonate; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; In methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1007/s00726-011-0912-4