4-(4-methoxy-benzyl)-5-oxo-3,4-diaza-bicyclo[4.1.0]hept-2-en-2-yl trifluoro-methanesulphonate

Base Information

Chemical Name:4-(4-methoxy-benzyl)-5-oxo-3,4-diaza-bicyclo[4.1.0]hept-2-en-2-yl trifluoro-methanesulphonate
CAS No.:1346701-78-7
Molecular Formula:C₁₄H₁₃F₃N₂O₅S
Molecular Weight:378.329
Hs Code.:

Synonyms:4-(4-methoxy-benzyl)-5-oxo-3,4-diaza-bicyclo[4.1.0]hept-2-en-2-yl trifluoro-methanesulphonate

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Chemical Property of 4-(4-methoxy-benzyl)-5-oxo-3,4-diaza-bicyclo[4.1.0]hept-2-en-2-yl trifluoro-methanesulphonate

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Technology Process of 4-(4-methoxy-benzyl)-5-oxo-3,4-diaza-bicyclo[4.1.0]hept-2-en-2-yl trifluoro-methanesulphonate

There total 3 articles about 4-(4-methoxy-benzyl)-5-oxo-3,4-diaza-bicyclo[4.1.0]hept-2-en-2-yl trifluoro-methanesulphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.8%

: 358-23-6
trifluoromethylsulfonic anhydride

: 154186-47-7
(+/-)-3-(4-methoxybenzyl)-3,4-diazabicyclo[4.1.0]heptane-2,5-dione

: 1346701-78-7
4-(4-methoxy-benzyl)-5-oxo-3,4-diaza-bicyclo[4.1.0]hept-2-en-2-yl trifluoro-methanesulphonate

Guidance literature:: With triethylamine; In dichloromethane; at -30 ℃; for 0.25h;

Reference yield:

: 5617-74-3
3-oxabicyclo[3.1.0]hexane-2,4-dione

: 1346701-78-7
4-(4-methoxy-benzyl)-5-oxo-3,4-diaza-bicyclo[4.1.0]hept-2-en-2-yl trifluoro-methanesulphonate

Guidance literature:: Multi-step reaction with 2 steps

1: acetonitrile / Reflux

2: triethylamine / dichloromethane / 0.25 h / -30 °C

With triethylamine; In dichloromethane; acetonitrile;

Reference yield:

: 140-69-2
4-methoxybenzylhydrazine

: 1346701-78-7
4-(4-methoxy-benzyl)-5-oxo-3,4-diaza-bicyclo[4.1.0]hept-2-en-2-yl trifluoro-methanesulphonate

Guidance literature:: Multi-step reaction with 2 steps

1: acetonitrile / Reflux

2: triethylamine / dichloromethane / 0.25 h / -30 °C

With triethylamine; In dichloromethane; acetonitrile;