C₄₄H₄₄O₁₀

Base Information

Chemical Name:C₄₄H₄₄O₁₀
CAS No.:1361049-68-4
Molecular Formula:C₄₄H₄₄O₁₀
Molecular Weight:732.827
Hs Code.:

C<sub>44</sub>H<sub>44</sub>O<sub>10</sub>

Synonyms:C₄₄H₄₄O₁₀

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Chemical Property of C₄₄H₄₄O₁₀

Chemical Property:

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Technology Process of C₄₄H₄₄O₁₀

There total 19 articles about C₄₄H₄₄O₁₀ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₄₄H₄₆O₁₀

: 1361049-68-4
C₄₄H₄₄O₁₀

Guidance literature:: With sodium hydrogencarbonate; Dess-Martin periodane; In dichloromethane; at 20 ℃; for 4h;
DOI:10.1002/anie.201106889

Reference yield:

: 1361049-72-0
(5R,2'R)-3-(benzyloxy)-5-[2'-(tert-butyldimethylsilyloxy)but-3'-enyl]-4-(methoxycarbonyl)furan-2(5H)-one

: 1361049-68-4
C₄₄H₄₄O₁₀

Guidance literature:: Multi-step reaction with 10 steps

1.1: barium hydroxide octahydrate / tetrahydrofuran; water / 60 h / 20 °C

2.1: 4-methyl-morpholine; methyl chloroformate / tetrahydrofuran / 0.5 h / -10 °C

2.2: 0.5 h / 0 °C

3.1: dmap; triethylamine / dichloromethane / 1.5 h / 0 - 20 °C

4.1: acetone; acetonitrile / 2 h / Irradiation

4.2: 16 h / 20 °C / 760.05 Torr

5.1: t-butyldimethylsiyl triflate / hexane; dichloromethane / 12 h / 0 °C / Molecular sieve

6.1: tetrahydrofuran; diethyl ether / -78 °C

7.1: pyridinium p-toluenesulfonate / dichloromethane / 3 h / 20 °C

8.1: dmap; triethylamine / 18 h / 20 °C

9.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 2 h / 20 °C

10.1: sodium hydrogencarbonate; Dess-Martin periodane / dichloromethane / 4 h / 20 °C

With 4-methyl-morpholine; dmap; barium hydroxide octahydrate; t-butyldimethylsiyl triflate; tetrabutyl ammonium fluoride; pyridinium p-toluenesulfonate; sodium hydrogencarbonate; Dess-Martin periodane; triethylamine; methyl chloroformate; In tetrahydrofuran; diethyl ether; hexane; dichloromethane; water; acetone; acetonitrile;
DOI:10.1002/anie.201106889

Reference yield:

: 1361049-71-9
C₁₆H₂₆O₆Si

: 1361049-68-4
C₄₄H₄₄O₁₀

Guidance literature:: Multi-step reaction with 11 steps

1.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 1 h / 0 - 20 °C

1.2: 21 h / 20 °C

2.1: barium hydroxide octahydrate / tetrahydrofuran; water / 60 h / 20 °C

3.1: 4-methyl-morpholine; methyl chloroformate / tetrahydrofuran / 0.5 h / -10 °C

3.2: 0.5 h / 0 °C

4.1: dmap; triethylamine / dichloromethane / 1.5 h / 0 - 20 °C

5.1: acetone; acetonitrile / 2 h / Irradiation

5.2: 16 h / 20 °C / 760.05 Torr

6.1: t-butyldimethylsiyl triflate / hexane; dichloromethane / 12 h / 0 °C / Molecular sieve

7.1: tetrahydrofuran; diethyl ether / -78 °C

8.1: pyridinium p-toluenesulfonate / dichloromethane / 3 h / 20 °C

9.1: dmap; triethylamine / 18 h / 20 °C

10.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 2 h / 20 °C

11.1: sodium hydrogencarbonate; Dess-Martin periodane / dichloromethane / 4 h / 20 °C

With 4-methyl-morpholine; dmap; barium hydroxide octahydrate; t-butyldimethylsiyl triflate; tetrabutyl ammonium fluoride; pyridinium p-toluenesulfonate; sodium hydride; sodium hydrogencarbonate; Dess-Martin periodane; triethylamine; methyl chloroformate; In tetrahydrofuran; diethyl ether; hexane; dichloromethane; water; N,N-dimethyl-formamide; acetone; acetonitrile; mineral oil;
DOI:10.1002/anie.201106889