ethyl 1-ethynylcyclohexyl carbonate

Base Information

Chemical Name:ethyl 1-ethynylcyclohexyl carbonate
CAS No.:95174-35-9
Molecular Formula:C₁₁H₁₆O₃
Molecular Weight:196.246
Hs Code.:

Synonyms:ethyl 1-ethynylcyclohexyl carbonate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of ethyl 1-ethynylcyclohexyl carbonate

Chemical Property:

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Technology Process of ethyl 1-ethynylcyclohexyl carbonate

There total 2 articles about ethyl 1-ethynylcyclohexyl carbonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 541-41-3
chloroformic acid ethyl ester

: 78-27-3
1-Ethynylcyclohexan-1-ol

: 95174-35-9
ethyl 1-ethynylcyclohexyl carbonate

Guidance literature:: 1-Ethynylcyclohexan-1-ol; With sodium hydride; In N,N-dimethyl-formamide; for 0.166667h; Cooling with ice;

chloroformic acid ethyl ester; In N,N-dimethyl-formamide; at 20 ℃;
DOI:10.3762/bjoc.12.197

Reference yield:

: 95174-35-9
ethyl 1-ethynylcyclohexyl carbonate

Guidance literature:: Na-<1-ethinyl-cyclohexanolat> in Bzl., Chlorameisensaeureethylester;

Reference yield: 95.0%

: 95174-35-9
ethyl 1-ethynylcyclohexyl carbonate

: 18107-18-1
diazomethyl-trimethyl-silane

: 1446452-02-3
C₁₂H₁₈O₃

Guidance literature:: With styrene; chloro(1,5-cyclooctadiene)(pentamethylcyclopentadiene)ruthenium(II); In methanol; diethyl ether; at 20 ℃; for 2h; Schlenk technique; Inert atmosphere;
DOI:10.1002/chem.201203796