alpha,alpha-dimethyl-3-(7-chloro-8-methyl-8H-imidazo[4,5-d]thiazolo[5,4-b]pyridin-2-yl)-benzeneacetic acid ethyl ester

Base Information

• Chemical Name: alpha,alpha-dimethyl-3-(7-chloro-8-methyl-8H-imidazo[4,5-d]thiazolo[5,4-b]pyridin-2-yl)-benzeneacetic acid ethyl ester
• CAS No.: 887254-73-1
• Molecular Formula: C₂₀H₁₉ClN₄O₂S
• Molecular Weight: 414.915

Synonyms:alpha,alpha-dimethyl-3-(7-chloro-8-methyl-8H-imidazo[4,5-d]thiazolo[5,4-b]pyridin-2-yl)-benzeneacetic acid ethyl ester

Chemical Property of alpha,alpha-dimethyl-3-(7-chloro-8-methyl-8H-imidazo[4,5-d]thiazolo[5,4-b]pyridin-2-yl)-benzeneacetic acid ethyl ester

Chemical Property:

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Technology Process of alpha,alpha-dimethyl-3-(7-chloro-8-methyl-8H-imidazo[4,5-d]thiazolo[5,4-b]pyridin-2-yl)-benzeneacetic acid ethyl ester

There total 1 articles about alpha,alpha-dimethyl-3-(7-chloro-8-methyl-8H-imidazo[4,5-d]thiazolo[5,4-b]pyridin-2-yl)-benzeneacetic acid ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

7-chloro-4-methyl-2-bromo-4H-imidazo[4,5-d]thiazolo[5,4-b]-pyridine (805319-85-1) + ethyl 2-(3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)-2-methylpropanoate (887254-78-6) → alpha,alpha-dimethyl-3-(7-chloro-8-methyl-8H-imidazo[4,5-d]thiazolo[5,4-b]pyridin-2-yl)-benzeneacetic acid ethyl ester (887254-73-1)

Guidance literature:

With potassium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In 1,2-dimethoxyethane; water; at 120 ℃; for 16h;

Reference yield:

alpha,alpha-dimethyl-3-(7-chloro-8-methyl-8H-imidazo[4,5-d]thiazolo[5,4-b]pyridin-2-yl)-benzeneacetic acid ethyl ester (887254-73-1) → C20H20N4O2S

Guidance literature:

With ammonium formate; palladium 10% on activated carbon; In isopropyl alcohol; at 65 ℃; for 4h;

upstream raw materials:

7-chloro-4-methyl-2-bromo-4H-imidazo[4,5-d]thiazolo[5,4-b]-pyridine

ethyl 2-(3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)-2-methylpropanoate

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