C₁₇H₂₆Br₂Si

Base Information

Chemical Name:C₁₇H₂₆Br₂Si
CAS No.:1448446-16-9
Molecular Formula:C₁₇H₂₆Br₂Si
Molecular Weight:418.287
Hs Code.:

C<sub>17</sub>H<sub>26</sub>Br<sub>2</sub>Si

Synonyms:C₁₇H₂₆Br₂Si

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Chemical Property of C₁₇H₂₆Br₂Si

Chemical Property:

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Technology Process of C₁₇H₂₆Br₂Si

There total 9 articles about C₁₇H₂₆Br₂Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 558-13-4
carbon tetrabromide

: 1448446-15-8
C₁₆H₂₆OSi

: 1448446-16-9
C₁₇H₂₆Br₂Si

Guidance literature:: With N-ethyl-N,N-diisopropylamine; triphenylphosphine; In dichloromethane; at -78 ℃; for 0.166667h; Inert atmosphere;
DOI:10.1002/anie.201209300

Reference yield:

: 1448446-13-6
C₂₂H₄₂OSi₂

: 1448446-16-9
C₁₇H₂₆Br₂Si

Guidance literature:: Multi-step reaction with 3 steps

1: hydrogenchloride / tetrahydrofuran; water / 0.25 h / 25 °C / Inert atmosphere

2: oxalyl dichloride; N-ethyl-N,N-diisopropylamine / dichloromethane; dimethyl sulfoxide / -78 °C / Inert atmosphere

3: N-ethyl-N,N-diisopropylamine; triphenylphosphine / dichloromethane / 0.17 h / -78 °C / Inert atmosphere

With hydrogenchloride; oxalyl dichloride; N-ethyl-N,N-diisopropylamine; triphenylphosphine; In tetrahydrofuran; dichloromethane; water; dimethyl sulfoxide;
DOI:10.1002/anie.201209300

Reference yield:

: 138124-05-7
(1S,6R)-(-)-8-Oxabicyclo<4.3.0>non-2-en-7-one

: 1448446-16-9
C₁₇H₂₆Br₂Si

Guidance literature:: Multi-step reaction with 7 steps

1.1: n-butyllithium; diisopropylamine / tetrahydrofuran; hexane / 0.5 h / -78 - -30 °C / Inert atmosphere

1.2: -78 °C / Inert atmosphere

2.1: diisobutylaluminium hydride / dichloromethane / 0.42 h / -78 °C / Inert atmosphere

3.1: n-butyllithium; diisopropylamine / diethyl ether; tetrahydrofuran; hexane / 0.33 h / -78 - -50 °C / Inert atmosphere

3.2: -78 - 25 °C / Inert atmosphere

4.1: n-butyllithium / tetrahydrofuran; hexane / 0.25 h / -78 °C / Inert atmosphere

4.2: -78 - 25 °C / Inert atmosphere

5.1: hydrogenchloride / tetrahydrofuran; water / 0.25 h / 25 °C / Inert atmosphere

6.1: oxalyl dichloride; N-ethyl-N,N-diisopropylamine / dichloromethane; dimethyl sulfoxide / -78 °C / Inert atmosphere

7.1: N-ethyl-N,N-diisopropylamine; triphenylphosphine / dichloromethane / 0.17 h / -78 °C / Inert atmosphere

With hydrogenchloride; n-butyllithium; oxalyl dichloride; diisobutylaluminium hydride; diisopropylamine; N-ethyl-N,N-diisopropylamine; triphenylphosphine; In tetrahydrofuran; diethyl ether; hexane; dichloromethane; water; dimethyl sulfoxide; 1.2: |Diels-Alder Cycloaddition;
DOI:10.1002/anie.201209300