N,N-diisopropyl-2-((2-methylphenyl)seleno)ferrocenecarboxamide

Base Information

Chemical Name:N,N-diisopropyl-2-((2-methylphenyl)seleno)ferrocenecarboxamide
CAS No.:875476-60-1
Molecular Formula:C₂₄H₂₉FeNOSe
Molecular Weight:482.307
Hs Code.:

Synonyms:N,N-diisopropyl-2-((2-methylphenyl)seleno)ferrocenecarboxamide

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Chemical Property of N,N-diisopropyl-2-((2-methylphenyl)seleno)ferrocenecarboxamide

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Technology Process of N,N-diisopropyl-2-((2-methylphenyl)seleno)ferrocenecarboxamide

There total 1 articles about N,N-diisopropyl-2-((2-methylphenyl)seleno)ferrocenecarboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 169830-46-0
[(bis(1-methylethyl)amino)carbonyl]ferrocene

: 69447-36-5
bis(2-methylphenyl) diselenide

: 875476-60-1
N,N-diisopropyl-2-((2-methylphenyl)seleno)ferrocenecarboxamide

Guidance literature:: With n-BuLi; Me₂NC₂H₄NC₂H₄; In diethyl ether; (N2); vac.-line technique; soln. of Fe complex in Et2O was added to mixt. of BuLi and (Me2NCH2)2 in Et2O; diselenide was added; stirred (-78°C, 30 min; room temp., 1 h); quenched with satd. NH4Cl; org. layer septd.; aq. layer extd. (Et2O); dried (Na2SO4); concd. (vac.); chromd. (petroleum ether/EtOAc, 18/2); recrystd. (CH2Cl2/hexane, 1/5); elem. anal.;
DOI:10.1021/om050353c

Reference yield:

: 875476-60-1
N,N-diisopropyl-2-((2-methylphenyl)seleno)ferrocenecarboxamide

: 7722-84-1
dihydrogen peroxide

: 875476-82-7
(N,N-diisopropylferrocenecarboxamide)Se(=O)(2-methylphenyl)

Guidance literature:: In methanol; mixt. of Fe complex and H2O2 (1.5 equiv.) in MeOH was reacted at 0°C; TLC monitoring; MnO2 added; stirred for 1 h; filtered; filtrate concd. (vac.);
DOI:10.1021/om050353c