N'''?{[(4?methylphenyl)sulfonyl]methyl}benzenecarboximidoyl isothiocyanate

Base Information

Chemical Name:N'''?{[(4?methylphenyl)sulfonyl]methyl}benzenecarboximidoyl isothiocyanate
CAS No.:127722-22-9
Molecular Formula:C₁₆H₁₄N₂O₂S₂
Molecular Weight:330.431
Hs Code.:

Synonyms:N'''?{[(4?methylphenyl)sulfonyl]methyl}benzenecarboximidoyl isothiocyanate

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Chemical Property of N'''?{[(4?methylphenyl)sulfonyl]methyl}benzenecarboximidoyl isothiocyanate

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Technology Process of N'''?{[(4?methylphenyl)sulfonyl]methyl}benzenecarboximidoyl isothiocyanate

There total 6 articles about N'''?{[(4?methylphenyl)sulfonyl]methyl}benzenecarboximidoyl isothiocyanate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 540-72-7
sodium thiocyanide

: 127722-21-8
N?{[(4?methylphenyl)sulfonyl]methyl}benzenecarboximidoyl chloride

: 127722-22-9
N'''?{[(4?methylphenyl)sulfonyl]methyl}benzenecarboximidoyl isothiocyanate

Guidance literature:: In acetonitrile; at 20 ℃; for 48h;
DOI:10.1007/s10822-021-00428-z

Reference yield:

: 14674-22-7
N?{[(4?methylphenyl)sulfonyl]methyl}benzamide

: 127722-22-9
N'''?{[(4?methylphenyl)sulfonyl]methyl}benzenecarboximidoyl isothiocyanate

Guidance literature:: Multi-step reaction with 2 steps

1: 83 percent / PCl₅ / benzene / 0.5 h / 60 - 80 °C

2: 80 percent / acetonitrile / 24 h / 20 - 25 °C

With phosphorus pentachloride; In acetonitrile; benzene;

Reference yield:

: 55-21-0,27208-38-4
benzamide

: 127722-22-9
N'''?{[(4?methylphenyl)sulfonyl]methyl}benzenecarboximidoyl isothiocyanate

Guidance literature:: Multi-step reaction with 3 steps

1: formic acid / water / 2.5 h / 75 - 85 °C

2: phosphorus pentachloride / benzene / 100 °C

3: acetonitrile / 48 h / 20 °C

With formic acid; phosphorus pentachloride; In water; acetonitrile; benzene;
DOI:10.1007/s10822-021-00428-z