Benzoic acid 3-[(E)-2-(3-benzyloxy-4-methoxy-phenyl)-vinyl]-5-methoxy-phenyl ester

Base Information

Chemical Name:Benzoic acid 3-[(E)-2-(3-benzyloxy-4-methoxy-phenyl)-vinyl]-5-methoxy-phenyl ester
CAS No.:76735-47-2
Molecular Formula:C₃₀H₂₆O₅
Molecular Weight:466.533
Hs Code.:

Synonyms:Benzoic acid 3-[(E)-2-(3-benzyloxy-4-methoxy-phenyl)-vinyl]-5-methoxy-phenyl ester

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Chemical Property of Benzoic acid 3-[(E)-2-(3-benzyloxy-4-methoxy-phenyl)-vinyl]-5-methoxy-phenyl ester

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:: SDS file from LookChem

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Technology Process of Benzoic acid 3-[(E)-2-(3-benzyloxy-4-methoxy-phenyl)-vinyl]-5-methoxy-phenyl ester

There total 10 articles about Benzoic acid 3-[(E)-2-(3-benzyloxy-4-methoxy-phenyl)-vinyl]-5-methoxy-phenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 76735-46-1,76735-60-9
3'-benzyloxy-5-hydroxy-3,4'-dimethoxystilbene

: 98-88-4
benzoyl chloride

: 76735-47-2
Benzoic acid 3-[(E)-2-(3-benzyloxy-4-methoxy-phenyl)-vinyl]-5-methoxy-phenyl ester

Guidance literature:: With pyridine; for 22h;

Reference yield:

: 6346-05-0
3-benzyloxy-4-methoxybenzaldehyde

: 76735-47-2
Benzoic acid 3-[(E)-2-(3-benzyloxy-4-methoxy-phenyl)-vinyl]-5-methoxy-phenyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 73 percent / 1.) n-butyl-lithium / tetrahydrofuran; hexane / 1.) 20 deg C, 90 min, 2.) 20 deg C, 18 h

2: 71 percent / pyridine / 22 h

With pyridine; n-butyllithium; In tetrahydrofuran; hexane;

Reference yield:

: 621-59-0
isovanillin

: 76735-47-2
Benzoic acid 3-[(E)-2-(3-benzyloxy-4-methoxy-phenyl)-vinyl]-5-methoxy-phenyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 84 percent / potassium carbonate, potassium iodide / acetone / 20 h / Heating

2: 73 percent / 1.) n-butyl-lithium / tetrahydrofuran; hexane / 1.) 20 deg C, 90 min, 2.) 20 deg C, 18 h

3: 71 percent / pyridine / 22 h

With pyridine; n-butyllithium; potassium carbonate; potassium iodide; In tetrahydrofuran; hexane; acetone;