Technology Process of C16H17N3O3
There total 3 articles about C16H17N3O3 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
tris-(dibenzylideneacetone)dipalladium(0); potassium carbonate; XPhos;
In
tert-butyl alcohol;
Reflux;
DOI:10.1016/j.bmcl.2014.03.026
- Guidance literature:
-
Multi-step reaction with 3 steps
1: thionyl chloride / dichloromethane / Reflux
2: triethylamine / dichloromethane / 20 °C
3: tris-(dibenzylideneacetone)dipalladium(0); XPhos; potassium carbonate / tert-butyl alcohol / Reflux
With
tris-(dibenzylideneacetone)dipalladium(0); thionyl chloride; potassium carbonate; triethylamine; XPhos;
In
dichloromethane; tert-butyl alcohol;
3: |Buchwald-Hartwig Coupling;
DOI:10.1016/j.bmcl.2014.03.026
- Guidance literature:
-
Multi-step reaction with 2 steps
1: triethylamine / dichloromethane / 20 °C
2: tris-(dibenzylideneacetone)dipalladium(0); XPhos; potassium carbonate / tert-butyl alcohol / Reflux
With
tris-(dibenzylideneacetone)dipalladium(0); potassium carbonate; triethylamine; XPhos;
In
dichloromethane; tert-butyl alcohol;
2: |Buchwald-Hartwig Coupling;
DOI:10.1016/j.bmcl.2014.03.026