Technology Process of C15H17(2)HO5
There total 10 articles about C15H17(2)HO5 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 10 steps
1: H+
2: PCC, NaOAc
3: D2O, pyridine
4: NaBH4 / ethanol
5: pyridine, DMAP
6: dimethylformamide
7: NaOMe / methanol
8: NaH, Bu4NI / tetrahydrofuran
9: H+ / methanol
10: Pb(OAc)4 / benzene
With
pyridine; lead(IV) acetate; dmap; sodium tetrahydroborate; water-d2; sodium methylate; sodium acetate; hydrogen cation; tetra-(n-butyl)ammonium iodide; sodium hydride; pyridinium chlorochromate;
In
tetrahydrofuran; methanol; ethanol; N,N-dimethyl-formamide; benzene;
DOI:10.1021/ja00020a059
- Guidance literature:
-
Multi-step reaction with 9 steps
1: PCC, NaOAc
2: D2O, pyridine
3: NaBH4 / ethanol
4: pyridine, DMAP
5: dimethylformamide
6: NaOMe / methanol
7: NaH, Bu4NI / tetrahydrofuran
8: H+ / methanol
9: Pb(OAc)4 / benzene
With
pyridine; lead(IV) acetate; dmap; sodium tetrahydroborate; water-d2; sodium methylate; sodium acetate; hydrogen cation; tetra-(n-butyl)ammonium iodide; sodium hydride; pyridinium chlorochromate;
In
tetrahydrofuran; methanol; ethanol; N,N-dimethyl-formamide; benzene;
DOI:10.1021/ja00020a059