C₃₂H₃₆N₄O₅S₂

Base Information

Chemical Name:C₃₂H₃₆N₄O₅S₂
CAS No.:1447194-84-4
Molecular Formula:C₃₂H₃₆N₄O₅S₂
Molecular Weight:620.794
Hs Code.:

C<sub>32</sub>H<sub>36</sub>N<sub>4</sub>O<sub>5</sub>S<sub>2</sub>

Synonyms:C₃₂H₃₆N₄O₅S₂

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₃₂H₃₆N₄O₅S₂

Chemical Property:

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Technology Process of C₃₂H₃₆N₄O₅S₂

There total 14 articles about C₃₂H₃₆N₄O₅S₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 54.0%

: 24424-99-5
di-tert-butyl dicarbonate

: 1447194-80-0
C₂₇H₂₈N₄O₃S₂

: 1447194-84-4
C₃₂H₃₆N₄O₅S₂

Guidance literature:: With 4-methyl-morpholine; In N,N-dimethyl-formamide; at 20 ℃;
DOI:10.1002/anie.201302106

Reference yield:

: 1447194-67-3
benzyl (4S)-4-(N-fmoc)-amino-3-oxopentanoate

: 1447194-84-4
C₃₂H₃₆N₄O₅S₂

Guidance literature:: Multi-step reaction with 6 steps

1: sulfuryl dichloride / dichloromethane / 1 h / 0 - 20 °C

2: ethanol / 40 °C

3: hydrogen; rosenmund catalyst / tetrahydrofuran; ethanol / 30 °C

4: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / dichloromethane / 4.5 h / 0 - 20 °C

5: diethylamine / d₇-N,N-dimethylformamide / 0.5 h / 20 °C

6: 4-methyl-morpholine / N,N-dimethyl-formamide / 20 °C

With 4-methyl-morpholine; sulfuryl dichloride; rosenmund catalyst; hydrogen; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; diethylamine; In tetrahydrofuran; ethanol; dichloromethane; d₇-N,N-dimethylformamide; N,N-dimethyl-formamide;
DOI:10.1002/anie.201302106

Reference yield:

: 35661-40-6
N-Fmoc L-Phe

: 1447194-84-4
C₃₂H₃₆N₄O₅S₂

Guidance literature:: Multi-step reaction with 9 steps

1: hydrogenchloride; 4-methyl-morpholine; (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate / dichloromethane

2: lithium aluminium tetrahydride / tetrahydrofuran / -25 °C

3: tin(ll) chloride / dichloromethane

4: sulfuryl dichloride / dichloromethane / 1 h / 0 - 20 °C

5: ethanol / 40 °C

6: d₇-N,N-dimethylformamide; diethylamine / 0.5 h / 20 °C

7: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / dichloromethane / 4.5 h / 0 - 20 °C

8: diethylamine / d₇-N,N-dimethylformamide / 0.5 h / 20 °C

9: 4-methyl-morpholine / N,N-dimethyl-formamide / 20 °C

With 4-methyl-morpholine; hydrogenchloride; lithium aluminium tetrahydride; sulfuryl dichloride; (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; diethylamine; tin(ll) chloride; In tetrahydrofuran; ethanol; dichloromethane; d₇-N,N-dimethylformamide; diethylamine; N,N-dimethyl-formamide;
DOI:10.1002/anie.201302106