2-(2-Benzoyl-1-cyan-1,2-dihydro-1-isochinolylmethyl)-benzoesaeureethylester

Base Information

Chemical Name:2-(2-Benzoyl-1-cyan-1,2-dihydro-1-isochinolylmethyl)-benzoesaeureethylester
CAS No.:145103-19-1
Molecular Formula:C₂₇H₂₂N₂O₃
Molecular Weight:422.483
Hs Code.:

Synonyms:2-(2-Benzoyl-1-cyan-1,2-dihydro-1-isochinolylmethyl)-benzoesaeureethylester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-(2-Benzoyl-1-cyan-1,2-dihydro-1-isochinolylmethyl)-benzoesaeureethylester

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Technology Process of 2-(2-Benzoyl-1-cyan-1,2-dihydro-1-isochinolylmethyl)-benzoesaeureethylester

There total 2 articles about 2-(2-Benzoyl-1-cyan-1,2-dihydro-1-isochinolylmethyl)-benzoesaeureethylester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 844-25-7,55839-33-3
2-benzoyl-1-cyano-1,2-dihydroisoquinoline

: 7115-91-5
2-ethoxycarbonylbenzyl bromide

: 145103-19-1
2-(2-Benzoyl-1-cyan-1,2-dihydro-1-isochinolylmethyl)-benzoesaeureethylester

Guidance literature:: With sodium hydroxide; cetyltrimethylammonim bromide; In benzene; for 20h;
DOI:10.1007/BF00811549

Reference yield:

: 87-24-1
ethyl 2-methylbenzoate

: 145103-19-1
2-(2-Benzoyl-1-cyan-1,2-dihydro-1-isochinolylmethyl)-benzoesaeureethylester

Guidance literature:: Multi-step reaction with 2 steps

1: 93 percent / N-bromosuccinimide, benzoyl peroxide (wet) / CCl₄ / 2 h / Heating

2: 80 percent / cetrimonium bromide, 50percent aq. NaOH / benzene / 20 h

With sodium hydroxide; N-Bromosuccinimide; Perbenzoic acid; cetyltrimethylammonim bromide; In tetrachloromethane; benzene;
DOI:10.1007/BF00811549