N'-(1,3-dioxoisoindolin-2-yl)-2-(4-mesityl-1-oxophthalazin-2(1H)-yl)acetamide

Base Information

Chemical Name:N'-(1,3-dioxoisoindolin-2-yl)-2-(4-mesityl-1-oxophthalazin-2(1H)-yl)acetamide
CAS No.:1374218-34-4
Molecular Formula:C₂₇H₂₂N₄O₄
Molecular Weight:466.496
Hs Code.:

Synonyms:N'-(1,3-dioxoisoindolin-2-yl)-2-(4-mesityl-1-oxophthalazin-2(1H)-yl)acetamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N'-(1,3-dioxoisoindolin-2-yl)-2-(4-mesityl-1-oxophthalazin-2(1H)-yl)acetamide

Chemical Property:

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Technology Process of N'-(1,3-dioxoisoindolin-2-yl)-2-(4-mesityl-1-oxophthalazin-2(1H)-yl)acetamide

There total 6 articles about N'-(1,3-dioxoisoindolin-2-yl)-2-(4-mesityl-1-oxophthalazin-2(1H)-yl)acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 85-44-9
phthalic anhydride

: 1374218-14-0
[4-(2,4,6-trimethylphenyl)-1(2H)-oxo-phthalazin-2-yl]acetic acid hydrazide

: 1374218-34-4
N'-(1,3-dioxoisoindolin-2-yl)-2-(4-mesityl-1-oxophthalazin-2(1H)-yl)acetamide

Guidance literature:: In acetic acid; for 10h; Reflux;
DOI:10.1002/cjoc.201100256

Reference yield:

: 85-44-9
phthalic anhydride

: 1374218-34-4
N'-(1,3-dioxoisoindolin-2-yl)-2-(4-mesityl-1-oxophthalazin-2(1H)-yl)acetamide

Guidance literature:: Multi-step reaction with 5 steps

1: aluminum (III) chloride

2: hydrazine hydrate / ethanol / 2 h / Reflux

3: potassium carbonate / acetone / 30 h / Reflux

4: hydrazine hydrate / ethanol / 2 h / Reflux

5: acetic acid / 10 h / Reflux

With aluminum (III) chloride; potassium carbonate; hydrazine hydrate; In ethanol; acetic acid; acetone; 1: Friedel Crafts reaction;
DOI:10.1002/cjoc.201100256

Reference yield:

: 1374218-13-9
[4-(2,4,6-trimethylphenyl)-1(2H)-oxo-phthalazin-2-yl]acetic acid ethyl ester

: 1374218-34-4
N'-(1,3-dioxoisoindolin-2-yl)-2-(4-mesityl-1-oxophthalazin-2(1H)-yl)acetamide

Guidance literature:: Multi-step reaction with 2 steps

1: hydrazine hydrate / ethanol / 2 h / Reflux

2: acetic acid / 10 h / Reflux

With hydrazine hydrate; In ethanol; acetic acid;
DOI:10.1002/cjoc.201100256