[(2E)-2-((3R,5S)-3-{[tert-butyl(diphenyl)silyl]oxy}-5-fluoro-4-methylenecyclohexylidene)ethyl](diphenyl)phosphine oxide

Base Information

Chemical Name:[(2E)-2-((3R,5S)-3-{[tert-butyl(diphenyl)silyl]oxy}-5-fluoro-4-methylenecyclohexylidene)ethyl](diphenyl)phosphine oxide
CAS No.:1154607-72-3
Molecular Formula:C₃₇H₄₀FO₂PSi
Molecular Weight:594.781
Hs Code.:

Synonyms:[(2E)-2-((3R,5S)-3-{[tert-butyl(diphenyl)silyl]oxy}-5-fluoro-4-methylenecyclohexylidene)ethyl](diphenyl)phosphine oxide

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Chemical Property of [(2E)-2-((3R,5S)-3-{[tert-butyl(diphenyl)silyl]oxy}-5-fluoro-4-methylenecyclohexylidene)ethyl](diphenyl)phosphine oxide

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Technology Process of [(2E)-2-((3R,5S)-3-{[tert-butyl(diphenyl)silyl]oxy}-5-fluoro-4-methylenecyclohexylidene)ethyl](diphenyl)phosphine oxide

There total 1 articles about [(2E)-2-((3R,5S)-3-{[tert-butyl(diphenyl)silyl]oxy}-5-fluoro-4-methylenecyclohexylidene)ethyl](diphenyl)phosphine oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 1154607-70-1
(2E)-2-((3R,5S)-3-{[tert-butyl(diphenyl)silyl]oxy}-5-fluoro-4-methylenecyclohexylidene)ethanol

: 829-85-6
diphenylphosphane

: 1154607-72-3
[(2E)-2-((3R,5S)-3-{[tert-butyl(diphenyl)silyl]oxy}-5-fluoro-4-methylenecyclohexylidene)ethyl](diphenyl)phosphine oxide

Guidance literature:: (2E)-2-((3R,5S)-3-{[tert-butyl(diphenyl)silyl]oxy}-5-fluoro-4-methylenecyclohexylidene)ethanol; With bis(trichloromethyl) carbonate; triethylamine; In hexane; at 0 - 20 ℃; for 1.5h;

diphenylphosphane; With n-butyllithium; In tetrahydrofuran; hexane; at -60 ℃; for 1.08333h;

Reference yield:

: 1154607-72-3
[(2E)-2-((3R,5S)-3-{[tert-butyl(diphenyl)silyl]oxy}-5-fluoro-4-methylenecyclohexylidene)ethyl](diphenyl)phosphine oxide

: 81506-41-4
(1R,3aR,7aR)-1-{(1R)-1,5-dimethyl-5-[(trimethylsilyl)oxy]hexyl}-7a-methyloctahydro-4H-inden-4-one

: 1154606-26-4
(1R,3S,5E,7E,17β)-3-fluoro-17-[(1R)-5-hydroxy-1,5-dimethylhexyl]-2-methylene-9,10-secoestra-5,7-dien-1-ol

Guidance literature:: [(2E)-2-((3R,5S)-3-{[tert-butyl(diphenyl)silyl]oxy}-5-fluoro-4-methylenecyclohexylidene)ethyl](diphenyl)phosphine oxide; (1R,3aR,7aR)-1-{(1R)-1,5-dimethyl-5-[(trimethylsilyl)oxy]hexyl}-7a-methyloctahydro-4H-inden-4-one; With lithium hexamethyldisilazane; In tetrahydrofuran; at -78 - 0 ℃;

With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 20 ℃;