Technology Process of C30H42N2O6S2
There total 5 articles about C30H42N2O6S2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
C20H32N2O3S2; 4-(dimethoxymethyl)benzoic acid;
In
dichloromethane;
at 0 ℃;
for 0.333333h;
Cooling with ice;
With
dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride;
In
dichloromethane;
at 0 - 20 ℃;
for 14.5h;
DOI:10.1021/ol3027335
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: triethylamine / methanol / 18 h / 20 °C
2.1: triethylamine; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; dmap / dichloromethane / 13 h / 0 - 20 °C / Cooling with ice
3.1: trifluoroacetic acid / dichloromethane / 4.5 h / 0 - 20 °C
4.1: dichloromethane / 0.33 h / 0 °C / Cooling with ice
4.2: 14.5 h / 0 - 20 °C
With
dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; trifluoroacetic acid;
In
methanol; dichloromethane;
DOI:10.1021/ol3027335
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: triethylamine / methanol / 18 h / 20 °C
2.1: triethylamine; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; dmap / dichloromethane / 13 h / 0 - 20 °C / Cooling with ice
3.1: trifluoroacetic acid / dichloromethane / 4.5 h / 0 - 20 °C
4.1: dichloromethane / 0.33 h / 0 °C / Cooling with ice
4.2: 14.5 h / 0 - 20 °C
With
dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; trifluoroacetic acid;
In
methanol; dichloromethane;
DOI:10.1021/ol3027335
