ethyl 5-(phenylthio)-1-((2-(trimethylsilyl)ethoxy)methyl)-1H-pyrazole-3-carboxylate

Base Information

Chemical Name:ethyl 5-(phenylthio)-1-((2-(trimethylsilyl)ethoxy)methyl)-1H-pyrazole-3-carboxylate
CAS No.:1174231-64-1
Molecular Formula:C₁₈H₂₆N₂O₃SSi
Molecular Weight:378.568
Hs Code.:

Synonyms:ethyl 5-(phenylthio)-1-((2-(trimethylsilyl)ethoxy)methyl)-1H-pyrazole-3-carboxylate

Suppliers and Price of ethyl 5-(phenylthio)-1-((2-(trimethylsilyl)ethoxy)methyl)-1H-pyrazole-3-carboxylate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of ethyl 5-(phenylthio)-1-((2-(trimethylsilyl)ethoxy)methyl)-1H-pyrazole-3-carboxylate

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of ethyl 5-(phenylthio)-1-((2-(trimethylsilyl)ethoxy)methyl)-1H-pyrazole-3-carboxylate

There total 1 articles about ethyl 5-(phenylthio)-1-((2-(trimethylsilyl)ethoxy)methyl)-1H-pyrazole-3-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 133560-59-5
5-phenylthio-1-<2-(trimethylsilyl)ethoxy>methyl-1H-pyrazole

: 623-49-4
ethyl cyanoformate

: 1174231-64-1
ethyl 5-(phenylthio)-1-((2-(trimethylsilyl)ethoxy)methyl)-1H-pyrazole-3-carboxylate

Guidance literature:: 5-phenylthio-1-<2-(trimethylsilyl)ethoxy>methyl-1H-pyrazole; With 2,2,6,6-tetramethyl-piperidyl-MgCl*LiCl; In tetrahydrofuran; at -15 ℃; for 10h; Inert atmosphere;

ethyl cyanoformate; In tetrahydrofuran; at -15 - 25 ℃; Inert atmosphere;
DOI:10.1021/ol901208d

Reference yield: 75.0%

: 1174231-64-1
ethyl 5-(phenylthio)-1-((2-(trimethylsilyl)ethoxy)methyl)-1H-pyrazole-3-carboxylate

: 106-95-6
allyl bromide

: 1174231-77-6
ethyl 4-allyl-5-(phenylthio)-1-(2-trimethylsilylethoxymethyl)-1H-pyrazole-3-carboxylate

Guidance literature:: ethyl 5-(phenylthio)-1-((2-(trimethylsilyl)ethoxy)methyl)-1H-pyrazole-3-carboxylate; With 2,2,6,6-tetramethyl-piperidyl-MgCl*LiCl; In tetrahydrofuran; at -30 ℃; for 2h; Inert atmosphere;

With copper(I) cyanide di(lithium chloride); In tetrahydrofuran; at -30 ℃; for 0.0833333h; Inert atmosphere;

allyl bromide; In tetrahydrofuran; at -30 - 25 ℃; Inert atmosphere;
DOI:10.1021/ol901208d