Methyl-carbamic acid 3-benzyl-5-methylcarbamoyloxymethyl-2-methylsulfanyl-3H-imidazol-4-ylmethyl ester

Base Information

Chemical Name:Methyl-carbamic acid 3-benzyl-5-methylcarbamoyloxymethyl-2-methylsulfanyl-3H-imidazol-4-ylmethyl ester
CAS No.:117120-86-2
Molecular Formula:C₁₇H₂₂N₄O₄S
Molecular Weight:378.452
Hs Code.:

Synonyms:Methyl-carbamic acid 3-benzyl-5-methylcarbamoyloxymethyl-2-methylsulfanyl-3H-imidazol-4-ylmethyl ester

Suppliers and Price of Methyl-carbamic acid 3-benzyl-5-methylcarbamoyloxymethyl-2-methylsulfanyl-3H-imidazol-4-ylmethyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of Methyl-carbamic acid 3-benzyl-5-methylcarbamoyloxymethyl-2-methylsulfanyl-3H-imidazol-4-ylmethyl ester

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of Methyl-carbamic acid 3-benzyl-5-methylcarbamoyloxymethyl-2-methylsulfanyl-3H-imidazol-4-ylmethyl ester

There total 3 articles about Methyl-carbamic acid 3-benzyl-5-methylcarbamoyloxymethyl-2-methylsulfanyl-3H-imidazol-4-ylmethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 624-83-9
methyl isocyanate

: 117121-03-6
(3-Benzyl-5-hydroxymethyl-2-methylsulfanyl-3H-imidazol-4-yl)-methanol

: 117120-86-2
Methyl-carbamic acid 3-benzyl-5-methylcarbamoyloxymethyl-2-methylsulfanyl-3H-imidazol-4-ylmethyl ester

Guidance literature:: With dibutyltin diacetate; In dichloromethane; for 3h; Ambient temperature;
DOI:10.1021/jm00121a023

Reference yield:

: 117121-00-3
diethyl 2-methylthio-4,5-imidazoledicarboxylate

: 117120-86-2
Methyl-carbamic acid 3-benzyl-5-methylcarbamoyloxymethyl-2-methylsulfanyl-3H-imidazol-4-ylmethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: NaH / dimethylformamide / 3 h / Ambient temperature

2: LiAlH₄ / CH₂Cl₂; diethyl ether / a) 0 - 5 deg C, 3 h, b) room temperature, 1 h

3: 75 percent / dibutyltin diacetate / CH₂Cl₂ / 3 h / Ambient temperature

With lithium aluminium tetrahydride; dibutyltin diacetate; sodium hydride; In diethyl ether; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jm00121a023

Reference yield:

: 1098-38-0
diethyl 1-benzyl-2-(methylthio)imidazole-4,5-dicarboxylate

: 117120-86-2
Methyl-carbamic acid 3-benzyl-5-methylcarbamoyloxymethyl-2-methylsulfanyl-3H-imidazol-4-ylmethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: LiAlH₄ / CH₂Cl₂; diethyl ether / a) 0 - 5 deg C, 3 h, b) room temperature, 1 h

2: 75 percent / dibutyltin diacetate / CH₂Cl₂ / 3 h / Ambient temperature

With lithium aluminium tetrahydride; dibutyltin diacetate; In diethyl ether; dichloromethane;
DOI:10.1021/jm00121a023