5,6-dihydro-5,5,6,6-tetramethyl-8-cyanodibenz-1,3-oxazonine

Base Information

• Chemical Name: 5,6-dihydro-5,5,6,6-tetramethyl-8-cyanodibenz-1,3-oxazonine
• CAS No.: 85696-86-2
• Molecular Formula: C₂₀H₂₀N₂O
• Molecular Weight: 304.392

Synonyms:5,6-dihydro-5,5,6,6-tetramethyl-8-cyanodibenz-1,3-oxazonine

Chemical Property of 5,6-dihydro-5,5,6,6-tetramethyl-8-cyanodibenz-1,3-oxazonine

Chemical Property:

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Technology Process of 5,6-dihydro-5,5,6,6-tetramethyl-8-cyanodibenz-1,3-oxazonine

There total 4 articles about 5,6-dihydro-5,5,6,6-tetramethyl-8-cyanodibenz-1,3-oxazonine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 18.0%

2-cyano-3,4-benzoquinoline N-oxide (27182-26-9) → 6(5H)-phenanthridinone (1015-89-0) + 6-(2-cyano-1,1,2-trimethylpropyloxy)phenanthridine (85696-85-1) + 5,6-dihydro-5,5,6,6-tetramethyl-8-cyanodibenz-1,3-oxazonine (85696-86-2) + phenanthridine-6-carbonitrile (2176-28-5)

Guidance literature:

In benzene; at 17 ℃; Further byproducts given; Irradiation; with Helios quartz light;

DOI:10.1039/P29880000235

Reference yield: 18.0%

2,3-Dimethyl-2-butene (563-79-1) + 2-cyano-3,4-benzoquinoline N-oxide (27182-26-9) → 6(5H)-phenanthridinone (1015-89-0) + 6-(2-cyano-1,1,2-trimethylpropyloxy)phenanthridine (85696-85-1) + 5,6-dihydro-5,5,6,6-tetramethyl-8-cyanodibenz-1,3-oxazonine (85696-86-2) + phenanthridine-6-carbonitrile (2176-28-5)

Guidance literature:

In benzene; Product distribution; Irradiation;

DOI:10.1016/S0040-4039(00)85730-5

Reference yield: 11.0%

2-cyano-3,4-benzoquinoline N-oxide (27182-26-9) + 2,3-Dimethyl-1-butene (563-78-0) → 6(5H)-phenanthridinone (1015-89-0) + 6-(2-cyano-1,1,2-trimethylpropyloxy)phenanthridine (85696-85-1) + 5,6-dihydro-5,5,6,6-tetramethyl-8-cyanodibenz-1,3-oxazonine (85696-86-2) + phenanthridine-6-carbonitrile (2176-28-5)

Guidance literature:

In benzene; at 17 ℃; Further byproducts given; Irradiation; with Helios quartz light;

DOI:10.1039/P29880000235

upstream raw materials:

2,3-Dimethyl-2-butene

2-cyano-3,4-benzoquinoline N-oxide

2,3-Dimethyl-1-butene

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