ISOAMYL NITRITE-15N

Base Information

• Chemical Name: ISOAMYL NITRITE-15N
• CAS No.: 120670-20-4
• Molecular Formula: C₅H₁₁NO₂
• Molecular Weight: 118.141
• Mol file: 120670-20-4.mol

Synonyms:Isoamylnitrite-15N

Chemical Property of ISOAMYL NITRITE-15N

Chemical Property:

• Refractive Index: n20/D 1.386(lit.)
• Boiling Point: 99 °C(lit.)
• Flash Point: 50 °F
• PSA: 38.66000
• Density: 0.879 g/mL at 25 °C(lit.)
• LogP: 1.73050

Purity/Quality:

99% ^*data from raw suppliers

Isoamyl nitrite-15N 98 atom % ^*data from reagent suppliers

Safty Information:

• Hazard Codes: F,Xn
• Statements: 11-20/22-36/37/38-43
• Safety Statements: 16-26-36

MSDS Files:

SDS file from LookChem

Useful:

• Uses: This product may be used as an analytical standard.

Technology Process of ISOAMYL NITRITE-15N

There total 2 articles about ISOAMYL NITRITE-15N which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

i-Amyl alcohol (123-51-3) → isoamyl 15N-nitrite (120670-20-4)

Guidance literature:

With sodium ⁽¹⁵⁾N-nitrite; sulfuric acid; for 1.5h;

Reference yield:

isopentyl nitrite (110-46-3) → isoamyl 15N-nitrite (120670-20-4)

Guidance literature:

With hydrogenchloride; sodium ⁽¹⁵⁾N-nitrite; In water; for 0.25h; cooling;

DOI:10.1021/jo702423z

upstream raw materials:

i-Amyl alcohol

isopentyl nitrite

Refernces

• 1、 Kurkovskaya, L. N.,Velezheva, V. S.,Sorokina, I. K.,Dmitrevskaya, L. I.,Zhil'nikov, V. G.. "SYNTHESIS OF 5-ARYL-4-(2-ACETYLAMINOBENZOYL)-1,2,3-TRIAZOLES WITH THE 15N ISOTOPE AT THE TERMINAL POSITIONS OF THE TRIAZOLE RINGS AND THEIR TAUTOMERIC COMPOSITION". . p. 1387 - 1392. Retrieved 2007/10/02.