C₂₅H₃₂O₂Si

Base Information

• Chemical Name: C₂₅H₃₂O₂Si
• CAS No.: 1456863-76-5
• Molecular Formula: C₂₅H₃₂O₂Si
• Molecular Weight: 392.613
• Mol file: 1456863-76-5.mol

Synonyms:C₂₅H₃₂O₂Si

Chemical Property of C₂₅H₃₂O₂Si

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₅H₃₂O₂Si

There total 1 articles about C₂₅H₃₂O₂Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

2-(tert-butyl-diphenyl-silanyloxymethyl)-cyclohex-2-enone + vinyl magnesium bromide (1826-67-1) → C25H32O2Si (1456863-76-5)

Guidance literature:

In tetrahydrofuran; at 0 ℃; for 1h;

DOI:10.1016/j.tetlet.2013.08.021

Reference yield: 83.0%

C25H32O2Si (1456863-76-5) + allyl bromide (106-95-6) → C28H36O2Si (1456863-77-6)

Guidance literature:

With potassium hydride; In tetrahydrofuran; at 0 ℃; for 1h;

DOI:10.1016/j.tetlet.2013.08.021

Reference yield:

C25H32O2Si (1456863-76-5) → C26H32O2Si (1456863-78-7)

Guidance literature:

Multi-step reaction with 2 steps

1: potassium hydride / tetrahydrofuran / 1 h / 0 °C

2: Grubbs catalyst first generation / dichloromethane / 2 h / 20 °C

With Grubbs catalyst first generation; potassium hydride; In tetrahydrofuran; dichloromethane;

DOI:10.1016/j.tetlet.2013.08.021

upstream raw materials:

vinyl magnesium bromide

Downstream raw materials:

C₂₆H₃₂O₂Si

C₂₆H₃₀O₃Si

C₂₈H₃₆O₂Si