non-8-ynoic acid chloride

Base Information

• Chemical Name: non-8-ynoic acid chloride
• CAS No.: 90675-38-0
• Molecular Formula: C₉H₁₃ClO
• Molecular Weight: 172.655
• Mol file: 90675-38-0.mol

Synonyms:non-8-ynoic acid chloride

Chemical Property of non-8-ynoic acid chloride

Chemical Property:

Purity/Quality:

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MSDS Files:

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Technology Process of non-8-ynoic acid chloride

There total 1 articles about non-8-ynoic acid chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

7-chloroheptanoic acid (821-57-8) → non-8-ynoic acid chloride (90675-38-0)

Guidance literature:

Multi-step reaction with 3 steps

1: NaI

2: Na, liq. NH₃

3: SOCl₂

With thionyl chloride; ammonia; sodium; sodium iodide;

Reference yield: 38.4%

non-8-ynoic acid chloride (90675-38-0) + 4,6-O-benzylidene-1-O-methyl-α-D-glucopyranoside (3162-96-7) → methyl 4,6-O-benzylidene-2-O-(8-nonynoyl)-α-D-glucopyranoside + methyl 4,6-O-benzylidene-3-O-(8-nonynoyl)-α-D-glucopyranoside + methyl 4,6-O-benzylidene-2,3-di-O-(8-nonynoyl)-α-D-glucopyranoside

Guidance literature:

With pyridine; In dichloromethane; at 20 ℃; for 24h;

DOI:10.1016/j.carres.2006.01.023

Reference yield:

non-8-ynoic acid chloride (90675-38-0) → 8-nonyn-1-ol (10160-28-8)

Guidance literature:

With lithium aluminium tetrahydride;

DOI:10.1007/BF00846495

upstream raw materials:

7-chloroheptanoic acid

Downstream raw materials:

8-nonyn-1-ol

non-8-ynyl 4-methylbenzenesulfonate