5-[3-(4-cyanobutyl)-5-benzoyl-2-imino-2,3-dihydro-1H-benzimidazol-1-yl]pentane nitrile

Base Information

Chemical Name:5-[3-(4-cyanobutyl)-5-benzoyl-2-imino-2,3-dihydro-1H-benzimidazol-1-yl]pentane nitrile
CAS No.:1441402-11-4
Molecular Formula:C₂₄H₂₅N₅O
Molecular Weight:399.495
Hs Code.:

Synonyms:5-[3-(4-cyanobutyl)-5-benzoyl-2-imino-2,3-dihydro-1H-benzimidazol-1-yl]pentane nitrile

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Chemical Property of 5-[3-(4-cyanobutyl)-5-benzoyl-2-imino-2,3-dihydro-1H-benzimidazol-1-yl]pentane nitrile

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Technology Process of 5-[3-(4-cyanobutyl)-5-benzoyl-2-imino-2,3-dihydro-1H-benzimidazol-1-yl]pentane nitrile

There total 4 articles about 5-[3-(4-cyanobutyl)-5-benzoyl-2-imino-2,3-dihydro-1H-benzimidazol-1-yl]pentane nitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 52329-60-9
(2-amino-1H-benzimidazol-5-yl)(phenyl)methanone

: 1441402-11-4
5-[3-(4-cyanobutyl)-5-benzoyl-2-imino-2,3-dihydro-1H-benzimidazol-1-yl]pentane nitrile

Guidance literature:: With tetrabutylammomium bromide; potassium carbonate; In acetonitrile; at 20 ℃;
DOI:10.1016/j.ejmech.2013.03.010

Reference yield:

: 39070-63-8
4-benzoylbenzene-1,2-diamine

: 1441402-11-4
5-[3-(4-cyanobutyl)-5-benzoyl-2-imino-2,3-dihydro-1H-benzimidazol-1-yl]pentane nitrile

Guidance literature:: Multi-step reaction with 4 steps

1: sodium hydroxide / ethanol; water / 3 h / Reflux

2: sodium hydroxide; potassium permanganate / water / 0.5 h / Reflux

3: ammonium hydroxide / 5 h / 145 - 150 °C

4: tetrabutylammomium bromide; potassium carbonate / acetonitrile / 20 °C

With ammonium hydroxide; potassium permanganate; tetrabutylammomium bromide; potassium carbonate; sodium hydroxide; In ethanol; water; acetonitrile;
DOI:10.1016/j.ejmech.2013.03.010

Reference yield:

: 92685-57-9
(2-mercapto-1H-benzo[d]imidazol-6-yl)(phenyl)methanone

: 1441402-11-4
5-[3-(4-cyanobutyl)-5-benzoyl-2-imino-2,3-dihydro-1H-benzimidazol-1-yl]pentane nitrile

Guidance literature:: Multi-step reaction with 3 steps

1: sodium hydroxide; potassium permanganate / water / 0.5 h / Reflux

2: ammonium hydroxide / 5 h / 145 - 150 °C

3: tetrabutylammomium bromide; potassium carbonate / acetonitrile / 20 °C

With ammonium hydroxide; potassium permanganate; tetrabutylammomium bromide; potassium carbonate; sodium hydroxide; In water; acetonitrile;
DOI:10.1016/j.ejmech.2013.03.010