N-butyl-N-[5-(4-methoxy-3,5-dimethylphenyl)-1,3,4-thiadiazol-2-yl]benzene-sulfonamide

Base Information

Chemical Name:N-butyl-N-[5-(4-methoxy-3,5-dimethylphenyl)-1,3,4-thiadiazol-2-yl]benzene-sulfonamide
CAS No.:1311285-91-2
Molecular Formula:C₂₁H₂₅N₃O₃S₂
Molecular Weight:431.58
Hs Code.:

Synonyms:N-butyl-N-[5-(4-methoxy-3,5-dimethylphenyl)-1,3,4-thiadiazol-2-yl]benzene-sulfonamide

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Chemical Property of N-butyl-N-[5-(4-methoxy-3,5-dimethylphenyl)-1,3,4-thiadiazol-2-yl]benzene-sulfonamide

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Technology Process of N-butyl-N-[5-(4-methoxy-3,5-dimethylphenyl)-1,3,4-thiadiazol-2-yl]benzene-sulfonamide

There total 3 articles about N-butyl-N-[5-(4-methoxy-3,5-dimethylphenyl)-1,3,4-thiadiazol-2-yl]benzene-sulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 5.0%

: 1220708-59-7
N-butyl-5-(4-methoxy-3,5-dimethylphenyl)-1,3,4-thiadiazol-2-amine

: 98-09-9
benzenesulfonyl chloride

: 1311285-91-2
N-butyl-N-[5-(4-methoxy-3,5-dimethylphenyl)-1,3,4-thiadiazol-2-yl]benzene-sulfonamide

Guidance literature:: With pyridine; dmap; at 110 ℃; for 0.5h; microwave irradiation;

Reference yield:

: 592-82-5
butyl isothiocyanate

: 1311285-91-2
N-butyl-N-[5-(4-methoxy-3,5-dimethylphenyl)-1,3,4-thiadiazol-2-yl]benzene-sulfonamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: hydrazine hydrate / methanol / 1 h / 10 - 15 °C

2.1: trichlorophosphate / 1,4-dioxane / 5 h / 80 °C

2.2: 0.5 h / 0 - 5 °C / pH 9 - 10

3.1: pyridine / dmap / 0.5 h / 110 °C / microwave irradiation

With pyridine; hydrazine hydrate; trichlorophosphate; dmap; In 1,4-dioxane; methanol;

Reference yield:

: 6610-31-7
4-butyl-3-thiosemicarbazide

: 1311285-91-2
N-butyl-N-[5-(4-methoxy-3,5-dimethylphenyl)-1,3,4-thiadiazol-2-yl]benzene-sulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: trichlorophosphate / 1,4-dioxane / 5 h / 80 °C

1.2: 0.5 h / 0 - 5 °C / pH 9 - 10

2.1: pyridine / dmap / 0.5 h / 110 °C / microwave irradiation

With pyridine; trichlorophosphate; dmap; In 1,4-dioxane;