(S) N-(4-methanesulphonylphenyl)-1-[3-phenyl-3-(4-methanesulphonylphenyl)-propyl]piperidin-4-yl acetamide

Base Information

Chemical Name:(S) N-(4-methanesulphonylphenyl)-1-[3-phenyl-3-(4-methanesulphonylphenyl)-propyl]piperidin-4-yl acetamide
CAS No.:718637-41-3
Molecular Formula:C₃₀H₃₆N₂O₅S₂
Molecular Weight:568.758
Hs Code.:

Synonyms:(S) N-(4-methanesulphonylphenyl)-1-[3-phenyl-3-(4-methanesulphonylphenyl)-propyl]piperidin-4-yl acetamide

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Chemical Property of (S) N-(4-methanesulphonylphenyl)-1-[3-phenyl-3-(4-methanesulphonylphenyl)-propyl]piperidin-4-yl acetamide

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Technology Process of (S) N-(4-methanesulphonylphenyl)-1-[3-phenyl-3-(4-methanesulphonylphenyl)-propyl]piperidin-4-yl acetamide

There total 6 articles about (S) N-(4-methanesulphonylphenyl)-1-[3-phenyl-3-(4-methanesulphonylphenyl)-propyl]piperidin-4-yl acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 527744-20-3
(S) 3-phenyl-3-(4-methanesulphonylphenyl)propionaldehyde

: N-(4-methanesulphonylphenyl)piperidin-4-yl acetamide

: 718637-41-3
(S) N-(4-methanesulphonylphenyl)-1-[3-phenyl-3-(4-methanesulphonylphenyl)-propyl]piperidin-4-yl acetamide

Guidance literature:: With sodium tris(acetoxy)borohydride; acetic acid; In dichloromethane; for 16h;

Reference yield:

: 718610-52-7
(E)-(4S,5R)-1-(3-[4-methanesulfonylphenyl]acryloyl)-3,4-dimethyl-5-phenyl-imidazolidin-2-one

: 718637-41-3
(S) N-(4-methanesulphonylphenyl)-1-[3-phenyl-3-(4-methanesulphonylphenyl)-propyl]piperidin-4-yl acetamide

Guidance literature:: Multi-step reaction with 4 steps

1.1: copper(l) iodide; N,N,N,N,-tetramethylethylenediamine / tetrahydrofuran / 0.17 h / 20 °C

1.2: 0.25 h / -78 °C

1.3: 18 h / 20 °C

2.1: lithium aluminium tetrahydride / tetrahydrofuran / 0.25 h / 0 °C

3.1: Dess-Martin periodinane / dichloromethane / 1.5 h / 20 °C

4.1: sodium tris(acetoxy)borohydride; acetic acid / dichloromethane / 16 h

With copper(l) iodide; lithium aluminium tetrahydride; Dess-Martin periodinane; N,N,N,N,-tetramethylethylenediamine; sodium tris(acetoxy)borohydride; acetic acid; In tetrahydrofuran; dichloromethane;

Reference yield:

: 718610-51-6
(4R,5S)-1-[(S)-3-(4-methanesulfonyl-phenyl)-3-phenyl-propionyl]-3,4-dimethyl-5-phenyl-imidazolidin-2-one

: 718637-41-3
(S) N-(4-methanesulphonylphenyl)-1-[3-phenyl-3-(4-methanesulphonylphenyl)-propyl]piperidin-4-yl acetamide

Guidance literature:: Multi-step reaction with 3 steps

1: lithium aluminium tetrahydride / tetrahydrofuran / 0.25 h / 0 °C

2: Dess-Martin periodinane / dichloromethane / 1.5 h / 20 °C

3: sodium tris(acetoxy)borohydride; acetic acid / dichloromethane / 16 h

With lithium aluminium tetrahydride; Dess-Martin periodinane; sodium tris(acetoxy)borohydride; acetic acid; In tetrahydrofuran; dichloromethane;