(CH(C₈H₄N(C₆H₄OMe))2)BF₂

Base Information

Chemical Name:(CH(C₈H₄N(C₆H₄OMe))2)BF₂
CAS No.:1323963-70-7
Molecular Formula:C₃₁H₂₃BF₂N₂O₂
Molecular Weight:504.344
Hs Code.:

(CH(C<sub>8</sub>H<sub>4</sub>N(C<sub>6</sub>H<sub>4</sub>OMe))2)BF<sub>2</sub>

Synonyms:(CH(C₈H₄N(C₆H₄OMe))2)BF₂

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Chemical Property of (CH(C₈H₄N(C₆H₄OMe))2)BF₂

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Technology Process of (CH(C₈H₄N(C₆H₄OMe))2)BF₂

There total 6 articles about (CH(C₈H₄N(C₆H₄OMe))2)BF₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 1322685-03-9
(MeOC₆H₄)C₈H₅NCHC₈H₄N(C₆H₄OMe)

: 109-63-7
boron trifluoride diethyl etherate

: 1323963-70-7
(CH(C₈H₄N(C₆H₄OMe))2)BF₂

Guidance literature:: With triethylamine; In toluene; at 80 - 100 ℃; for 3h; Inert atmosphere;

Reference yield: 81.0%

: C₃₁H₂₄N₂O₂

: 1323963-70-7
(CH(C₈H₄N(C₆H₄OMe))2)BF₂

Guidance literature:: With boron trifluoride diethyl etherate; triethylamine; In dichloromethane; at 50 ℃; for 16h;
DOI:10.1039/c3tc30276h

Reference yield: 81.0%

: 1322685-03-9
(MeOC₆H₄)C₈H₅NCHC₈H₄N(C₆H₄OMe)

: 109-63-7
trifluoroborane diethyl ether

: 1323963-70-7
(CH(C₈H₄N(C₆H₄OMe))2)BF₂

Guidance literature:: With N(CH₂CH₃)3; In dichloromethane; addn. of dry triethylamine to CH2Cl2 soln. of bis(iso)indomethene deriv., addn. of boron compd., stirring at 50°C for 16 h; washing with water, separating organic layer, drying over MgSO4, concg.,chromy. (silica gel, CHCl3), elem. anal.;
DOI:10.1246/bcsj.20100340