((3-(4-(((2-(3-(((tert-butoxy)carbonyl)amino)propoxy)benzoyl)(6-phenoxy-2-benzothiazolyl)amino)methyl)phenoxy)propyl)carbonimidoyl)-bis-carbamic acid bis(tert-butyl) ester

Base Information

Chemical Name:((3-(4-(((2-(3-(((tert-butoxy)carbonyl)amino)propoxy)benzoyl)(6-phenoxy-2-benzothiazolyl)amino)methyl)phenoxy)propyl)carbonimidoyl)-bis-carbamic acid bis(tert-butyl) ester
CAS No.:754992-79-5
Molecular Formula:C₄₉H₆₀N₆O₁₀S
Molecular Weight:925.116
Hs Code.:

((3-(4-(((2-(3-(((tert-butoxy)carbonyl)amino)propoxy)benzoyl)(6-phenoxy-2-benzothiazolyl)amino)methyl)phenoxy)propyl)carbonimidoyl)-bis-carbamic acid bis(tert-butyl) ester

Synonyms:((3-(4-(((2-(3-(((tert-butoxy)carbonyl)amino)propoxy)benzoyl)(6-phenoxy-2-benzothiazolyl)amino)methyl)phenoxy)propyl)carbonimidoyl)-bis-carbamic acid bis(tert-butyl) ester

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Chemical Property of ((3-(4-(((2-(3-(((tert-butoxy)carbonyl)amino)propoxy)benzoyl)(6-phenoxy-2-benzothiazolyl)amino)methyl)phenoxy)propyl)carbonimidoyl)-bis-carbamic acid bis(tert-butyl) ester

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Purity/Quality:: 99% ^*data from raw suppliers

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Technology Process of ((3-(4-(((2-(3-(((tert-butoxy)carbonyl)amino)propoxy)benzoyl)(6-phenoxy-2-benzothiazolyl)amino)methyl)phenoxy)propyl)carbonimidoyl)-bis-carbamic acid bis(tert-butyl) ester

There total 9 articles about ((3-(4-(((2-(3-(((tert-butoxy)carbonyl)amino)propoxy)benzoyl)(6-phenoxy-2-benzothiazolyl)amino)methyl)phenoxy)propyl)carbonimidoyl)-bis-carbamic acid bis(tert-butyl) ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 73279-02-4
2-[3-[4-Formylphenoxy]propyl]-1H-isoindole-1,3-dione

: 754992-79-5
((3-(4-(((2-(3-(((tert-butoxy)carbonyl)amino)propoxy)benzoyl)(6-phenoxy-2-benzothiazolyl)amino)methyl)phenoxy)propyl)carbonimidoyl)-bis-carbamic acid bis(tert-butyl) ester

Guidance literature:: Multi-step reaction with 5 steps

1: molecular sieves 4 Angstroem / toluene / Heating

2: 0.77 g / NaBH₄ / toluene; ethanol / Heating

3: 45 percent / diisopropylethylamine / tetrahydrofuran; CH₂Cl₂ / 60 °C

4: hydrazine hydrate / ethanol / 68 °C

5: 0.174 g / CH₂Cl₂ / 20 °C

With sodium tetrahydroborate; 4 A molecular sieve; hydrazine hydrate; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; ethanol; dichloromethane; toluene;
DOI:10.1016/j.bmc.2004.05.040

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 754992-79-5
((3-(4-(((2-(3-(((tert-butoxy)carbonyl)amino)propoxy)benzoyl)(6-phenoxy-2-benzothiazolyl)amino)methyl)phenoxy)propyl)carbonimidoyl)-bis-carbamic acid bis(tert-butyl) ester

Guidance literature:: Multi-step reaction with 7 steps

1: 91 percent / triethylamine / methanol; acetonitrile / 1.5 h / 20 °C

2: 70 percent / K₂CO₃ / dimethylformamide / 24 h / 50 °C

3: 93 percent / NaOH / methanol; H₂O / 6 h / Heating

4: 90 percent / diethylaminosulfur trifluoride / CH₂Cl₂ / 25 °C

5: 45 percent / diisopropylethylamine / tetrahydrofuran; CH₂Cl₂ / 60 °C

6: hydrazine hydrate / ethanol / 68 °C

7: 0.174 g / CH₂Cl₂ / 20 °C

With sodium hydroxide; diethylamino-sulfur trifluoride; potassium carbonate; hydrazine hydrate; triethylamine; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; methanol; ethanol; dichloromethane; water; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1016/j.bmc.2004.05.040

Reference yield:

: 123-08-0,65581-83-1
4-hydroxy-benzaldehyde

: 754992-79-5
((3-(4-(((2-(3-(((tert-butoxy)carbonyl)amino)propoxy)benzoyl)(6-phenoxy-2-benzothiazolyl)amino)methyl)phenoxy)propyl)carbonimidoyl)-bis-carbamic acid bis(tert-butyl) ester

Guidance literature:: Multi-step reaction with 6 steps

1: 68 percent / K₂CO₃ / acetonitrile / 15 h / 20 °C

2: molecular sieves 4 Angstroem / toluene / Heating

3: 0.77 g / NaBH₄ / toluene; ethanol / Heating

4: 45 percent / diisopropylethylamine / tetrahydrofuran; CH₂Cl₂ / 60 °C

5: hydrazine hydrate / ethanol / 68 °C

6: 0.174 g / CH₂Cl₂ / 20 °C

With sodium tetrahydroborate; 4 A molecular sieve; potassium carbonate; hydrazine hydrate; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; ethanol; dichloromethane; toluene; acetonitrile;
DOI:10.1016/j.bmc.2004.05.040