Technology Process of C17H26O4Si
There total 1 articles about C17H26O4Si which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
trimethyl phosphonoacetate;
With
lithium bromide;
In
tetrahydrofuran;
at 23 ℃;
for 0.25h;
Inert atmosphere;
With
triethylamine;
In
tetrahydrofuran;
at 23 ℃;
for 0.25h;
Inert atmosphere;
3-[(tert-butyldimethylsilyl)oxy]-2-methoxybenzaldehyde;
In
tetrahydrofuran;
at 23 ℃;
for 5h;
Inert atmosphere;
DOI:10.1002/ejoc.201001281
- Guidance literature:
-
With
palladium 10% on activated carbon; hydrogen;
In
methanol;
at 23 ℃;
for 0.5h;
DOI:10.1002/ejoc.201001281
- Guidance literature:
-
Multi-step reaction with 3 steps
1: palladium 10% on activated carbon; hydrogen / methanol / 0.5 h / 23 °C
2: diisobutylaluminium hydride / dichloromethane; toluene / 1.5 h / -78 °C / Inert atmosphere
3: tetrahydrofuran / 2 h / -78 - 23 °C / Inert atmosphere
With
palladium 10% on activated carbon; hydrogen; diisobutylaluminium hydride;
In
tetrahydrofuran; methanol; dichloromethane; toluene;
DOI:10.1002/ejoc.201001281