(S)-3-benzyl-N-(t-butoxycarbonyl)-N-(4-methoxyphenyl)-(Z)-1-buten-1-amine

Base Information

• Chemical Name: (S)-3-benzyl-N-(t-butoxycarbonyl)-N-(4-methoxyphenyl)-(Z)-1-buten-1-amine
• CAS No.: 501032-61-7
• Molecular Formula: C₂₃H₂₉NO₃
• Molecular Weight: 367.488

Synonyms:(S)-3-benzyl-N-(t-butoxycarbonyl)-N-(4-methoxyphenyl)-(Z)-1-buten-1-amine

Chemical Property of (S)-3-benzyl-N-(t-butoxycarbonyl)-N-(4-methoxyphenyl)-(Z)-1-buten-1-amine

Chemical Property:

Purity/Quality:

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Technology Process of (S)-3-benzyl-N-(t-butoxycarbonyl)-N-(4-methoxyphenyl)-(Z)-1-buten-1-amine

There total 1 articles about (S)-3-benzyl-N-(t-butoxycarbonyl)-N-(4-methoxyphenyl)-(Z)-1-buten-1-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

benzyl bromide (100-39-0) + N-(t-Butoxycarbonyl)-N-(4-methoxyphenyl)-(E)-2-buten-1-amine → N-(t-butoxycarbonyl)-N-(4-methoxyphenyl)-1-phenyl-(E)-3-penten-2-amine + (R)-3-benzyl-N-(t-butoxycarbonyl)-N-(4-methoxyphenyl)-(Z)-1-buten-1-amine + (S)-3-benzyl-N-(t-butoxycarbonyl)-N-(4-methoxyphenyl)-(Z)-1-buten-1-amine (501032-61-7) + (R)-3-benzyl-N-(t-butoxycarbonyl)-N-(4-methoxyphenyl)-(E)-1-buten-1-amine

Guidance literature:

N-(t-Butoxycarbonyl)-N-(4-methoxyphenyl)-(E)-2-buten-1-amine; With n-butyllithium; (-)-sparteine; In hexane; toluene; at -78 ℃;

benzyl bromide; In hexane; toluene; at -78 ℃; Further stages. Further byproducts. Title compound not separated from byproducts.;

DOI:10.1021/jo0260084

Reference yield:

(S)-3-benzyl-N-(t-butoxycarbonyl)-N-(4-methoxyphenyl)-(Z)-1-buten-1-amine (501032-61-7) → (S)-3-benzyl-N-(t-butoxycarbonyl)-N-(4-methoxyphenyl)-(E)-1-buten-1-amine

Guidance literature:

(S)-3-benzyl-N-(t-butoxycarbonyl)-N-(4-methoxyphenyl)-(Z)-1-buten-1-amine; With trifluoroacetic anhydride; In dichloromethane; at 20 ℃; for 0.166667h;

With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 1h; Further stages.;

DOI:10.1021/jo0260084

upstream raw materials:

benzyl bromide

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