allyl N-[2-((fluorenylmethoxycarbonyl)amino)ethyl]-N-[(N²,N²-bis(tert-butoxycarbonyl)-O⁶-benzylguanin-9-yl)acetyl]glycinate

Base Information

• Chemical Name: allyl N-[2-((fluorenylmethoxycarbonyl)amino)ethyl]-N-[(N²,N²-bis(tert-butoxycarbonyl)-O⁶-benzylguanin-9-yl)acetyl]glycinate
• CAS No.: 1028077-23-7
• Molecular Formula: C₄₆H₅₁N₇O₁₀
• Molecular Weight: 861.952

Synonyms:allyl N-[2-((fluorenylmethoxycarbonyl)amino)ethyl]-N-[(N²,N²-bis(tert-butoxycarbonyl)-O⁶-benzylguanin-9-yl)acetyl]glycinate

Chemical Property of allyl N-[2-((fluorenylmethoxycarbonyl)amino)ethyl]-N-[(N²,N²-bis(tert-butoxycarbonyl)-O⁶-benzylguanin-9-yl)acetyl]glycinate

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Technology Process of allyl N-[2-((fluorenylmethoxycarbonyl)amino)ethyl]-N-[(N²,N²-bis(tert-butoxycarbonyl)-O⁶-benzylguanin-9-yl)acetyl]glycinate

There total 1 articles about allyl N-[2-((fluorenylmethoxycarbonyl)amino)ethyl]-N-[(N²,N²-bis(tert-butoxycarbonyl)-O⁶-benzylguanin-9-yl)acetyl]glycinate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

[N2,N2-bis(tert-butoxycarbonyl)-O6-benzylguanidin-9-yl]acetic acid (1028077-17-9) + prop-2-en-1-yl 2-{[2-({[(9H-fluoren-9-yl)methoxy]carbonyl}amino)ethyl]amino}acetate (406683-69-0) → allyl N-[2-((fluorenylmethoxycarbonyl)amino)ethyl]-N-[(N2,N2-bis(tert-butoxycarbonyl)-O6-benzylguanin-9-yl)acetyl]glycinate (1028077-23-7)

Guidance literature:

With benzotriazol-1-ol; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; In dichloromethane; at 20 ℃; for 12h;

DOI:10.1021/jo800195j

Reference yield: 84.0%

allyl N-[2-((fluorenylmethoxycarbonyl)amino)ethyl]-N-[(N2,N2-bis(tert-butoxycarbonyl)-O6-benzylguanin-9-yl)acetyl]glycinate (1028077-23-7) → N-[2-((fluorenylmethoxycarbonyl)amino)ethyl]-N-[(N2,N2-bis(tert-butoxycarbonyl)-O6-benzylguanin-9-yl)acetyl]glycine (1028077-29-3)

Guidance literature:

With 4-methyl-morpholine; acetic acid; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In chloroform; for 12h;

DOI:10.1021/jo800195j

upstream raw materials:

[N²,N²-bis(tert-butoxycarbonyl)-O⁶-benzylguanidin-9-yl]acetic acid

prop-2-en-1-yl 2-{[2-({[(9H-fluoren-9-yl)methoxy]carbonyl}amino)ethyl]amino}acetate

Downstream raw materials:

N-[2-((fluorenylmethoxycarbonyl)amino)ethyl]-N-[(N²,N²-bis(tert-butoxycarbonyl)-O⁶-benzylguanin-9-yl)acetyl]glycine

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