(2R,5S)-2-((R)-1-(tert-butyldimethylsilyloxy)propan-2-yl)-5-methylcyclohexanone

Base Information

Chemical Name:(2R,5S)-2-((R)-1-(tert-butyldimethylsilyloxy)propan-2-yl)-5-methylcyclohexanone
CAS No.:1220706-70-6
Molecular Formula:C₁₆H₃₂O₂Si
Molecular Weight:284.514
Hs Code.:

Synonyms:(2R,5S)-2-((R)-1-(tert-butyldimethylsilyloxy)propan-2-yl)-5-methylcyclohexanone

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2R,5S)-2-((R)-1-(tert-butyldimethylsilyloxy)propan-2-yl)-5-methylcyclohexanone

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Technology Process of (2R,5S)-2-((R)-1-(tert-butyldimethylsilyloxy)propan-2-yl)-5-methylcyclohexanone

There total 1 articles about (2R,5S)-2-((R)-1-(tert-butyldimethylsilyloxy)propan-2-yl)-5-methylcyclohexanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 1220706-69-3
(1R,2R,5S)-2-((R)-1-(tert-butyldimethylsilyloxy)propan-2-yl)-5-methylcyclohexanol

: 1220706-70-6
(2R,5S)-2-((R)-1-(tert-butyldimethylsilyloxy)propan-2-yl)-5-methylcyclohexanone

Guidance literature:: With sodium acetate; pyridinium chlorochromate; In dichloromethane; at 10 ℃; Inert atmosphere;
DOI:10.1016/j.tet.2010.01.054

Reference yield: 87.0%

: 17640-15-2
methyl cyanoformate

: 1220706-70-6
(2R,5S)-2-((R)-1-(tert-butyldimethylsilyloxy)propan-2-yl)-5-methylcyclohexanone

: 1220706-67-1
methyl (3R,6S)-3-((R)-1-(tert-butyldimethylsilyloxy)propan-2-yl)-6-methyl-2-oxocyclohexanecarboxylate

Guidance literature:: (2R,5S)-2-((R)-1-(tert-butyldimethylsilyloxy)propan-2-yl)-5-methylcyclohexanone; With n-butyllithium; diisopropylamine; In tetrahydrofuran; hexane; at -78 ℃; Inert atmosphere;

methyl cyanoformate; In tetrahydrofuran; hexane; at -78 ℃; Inert atmosphere;
DOI:10.1016/j.tet.2010.01.054