(1R,2R,5S)-2-((R)-1-(tert-butyldimethylsilyloxy)propan-2-yl)-5-methylcyclohexanol

Base Information

Chemical Name:(1R,2R,5S)-2-((R)-1-(tert-butyldimethylsilyloxy)propan-2-yl)-5-methylcyclohexanol
CAS No.:1220706-69-3
Molecular Formula:C₁₆H₃₄O₂Si
Molecular Weight:286.53
Hs Code.:

Synonyms:(1R,2R,5S)-2-((R)-1-(tert-butyldimethylsilyloxy)propan-2-yl)-5-methylcyclohexanol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (1R,2R,5S)-2-((R)-1-(tert-butyldimethylsilyloxy)propan-2-yl)-5-methylcyclohexanol

Chemical Property:

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Technology Process of (1R,2R,5S)-2-((R)-1-(tert-butyldimethylsilyloxy)propan-2-yl)-5-methylcyclohexanol

There total 1 articles about (1R,2R,5S)-2-((R)-1-(tert-butyldimethylsilyloxy)propan-2-yl)-5-methylcyclohexanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 122517-60-6
(?)-neo-isopulegol

: 18162-48-6
tert-butyldimethylsilyl chloride

: 1220706-69-3
(1R,2R,5S)-2-((R)-1-(tert-butyldimethylsilyloxy)propan-2-yl)-5-methylcyclohexanol

: 1220706-81-9
(1R,2R,5S)-2-((S)-1-(tert-butyldimethylsilyloxy)propan-2-yl)-5-methylcyclohexanol

Guidance literature:: (?)-neo-isopulegol; With dimethylsulfide borane complex; In tetrahydrofuran; at 0 - 20 ℃; Inert atmosphere;

With dihydrogen peroxide; sodium hydroxide; In tetrahydrofuran; at 0 - 20 ℃;

tert-butyldimethylsilyl chloride; Further stages;
DOI:10.1016/j.tet.2010.01.054

Reference yield: 94.0%

: 1220706-69-3
(1R,2R,5S)-2-((R)-1-(tert-butyldimethylsilyloxy)propan-2-yl)-5-methylcyclohexanol

: 1220706-70-6
(2R,5S)-2-((R)-1-(tert-butyldimethylsilyloxy)propan-2-yl)-5-methylcyclohexanone

Guidance literature:: With sodium acetate; pyridinium chlorochromate; In dichloromethane; at 10 ℃; Inert atmosphere;
DOI:10.1016/j.tet.2010.01.054