1-O-benzyl-3-O-[(10RS)-10-methylheptadec-16-en-1-yl]-snglycerol

Base Information

Chemical Name:1-O-benzyl-3-O-[(10RS)-10-methylheptadec-16-en-1-yl]-snglycerol
CAS No.:1610613-85-8
Molecular Formula:C₂₈H₄₈O₃
Molecular Weight:432.687
Hs Code.:

Synonyms:1-O-benzyl-3-O-[(10RS)-10-methylheptadec-16-en-1-yl]-snglycerol

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Chemical Property of 1-O-benzyl-3-O-[(10RS)-10-methylheptadec-16-en-1-yl]-snglycerol

Chemical Property:

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Technology Process of 1-O-benzyl-3-O-[(10RS)-10-methylheptadec-16-en-1-yl]-snglycerol

There total 18 articles about 1-O-benzyl-3-O-[(10RS)-10-methylheptadec-16-en-1-yl]-snglycerol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 1610613-81-4
3-O-[(10RS)-10-methylheptadec-16-en-1-yl]-sn-glycerol

: 100-39-0
benzyl bromide

: 1610613-85-8
1-O-benzyl-3-O-[(10RS)-10-methylheptadec-16-en-1-yl]-snglycerol

Guidance literature:: 3-O-[(10RS)-10-methylheptadec-16-en-1-yl]-sn-glycerol; With di(n-butyl)tin oxide; In methanol; toluene; at 20 ℃; for 1h; Molecular sieve; Reflux;

benzyl bromide; In methanol; 1,2-dimethoxyethane; toluene; for 2.5h; Molecular sieve; Reflux;
DOI:10.1039/c4ob00048j

Reference yield:

: 4117-09-3
7-bromo-hept-1-ene

: 1610613-85-8
1-O-benzyl-3-O-[(10RS)-10-methylheptadec-16-en-1-yl]-snglycerol

Guidance literature:: Multi-step reaction with 11 steps

1.1: sodium hydride / toluene / 8 h / Reflux

2.1: potassium hydroxide / water; ethanol / 8 h / Reflux

3.1: Isopropylbenzene; pyridine / 1 h / Reflux

4.1: lithium aluminium tetrahydride / diethyl ether / 6 h / Reflux

5.1: pyridinium p-toluenesulfonate / dichloromethane

6.1: dibromotriphenylphosphorane / dichloromethane / 20 °C

7.1: magnesium / diethyl ether / 3 h / Reflux

7.2: 3 h / -3 - 0 °C

8.1: triphenylphosphine; bromine / dichloromethane / 0 - 20 °C

9.1: potassium hydride / toluene / 18 h / 20 °C

9.2: 10 h / Reflux

10.1: methanol; pyridinium p-toluenesulfonate / 10 h / Reflux

11.1: di(n-butyl)tin oxide / methanol; toluene / 1 h / 20 °C / Molecular sieve; Reflux

11.2: 2.5 h / Molecular sieve; Reflux

With pyridine; methanol; lithium aluminium tetrahydride; Isopropylbenzene; bromine; pyridinium p-toluenesulfonate; potassium hydride; sodium hydride; di(n-butyl)tin oxide; magnesium; triphenylphosphine; potassium hydroxide; dibromotriphenylphosphorane; In methanol; diethyl ether; ethanol; dichloromethane; water; toluene;
DOI:10.1039/c4ob00048j

Reference yield:

: 6-bromo-4-methyl-hexanal

: 1610613-85-8
1-O-benzyl-3-O-[(10RS)-10-methylheptadec-16-en-1-yl]-snglycerol

Guidance literature:: Multi-step reaction with 9 steps

1.1: sodium tetrahydroborate / methanol / 20 °C

2.1: pyridinium p-toluenesulfonate / dichloromethane / 18 h / 20 °C

3.1: magnesium / diethyl ether / 2 h / Reflux

3.2: -5 - 0 °C

4.1: triphenylphosphine; bromine / dichloromethane / 0 - 20 °C

5.1: magnesium / tetrahydrofuran

5.2: 0 °C

6.1: triphenylphosphine; bromine / dichloromethane / 0 - 20 °C

7.1: potassium hydride / toluene / 18 h / 20 °C

7.2: 10 h / Reflux

8.1: methanol; pyridinium p-toluenesulfonate / 10 h / Reflux

9.1: di(n-butyl)tin oxide / methanol; toluene / 1 h / 20 °C / Molecular sieve; Reflux

9.2: 2.5 h / Molecular sieve; Reflux

With methanol; sodium tetrahydroborate; bromine; pyridinium p-toluenesulfonate; potassium hydride; di(n-butyl)tin oxide; magnesium; triphenylphosphine; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; toluene;
DOI:10.1039/c4ob00048j