isopropyl 3-amino-2-(4-tert-butyl-2-nitrophenoxy)-5-[(diisopropylamino)carbonyl]benzoate

Base Information

Chemical Name:isopropyl 3-amino-2-(4-tert-butyl-2-nitrophenoxy)-5-[(diisopropylamino)carbonyl]benzoate
CAS No.:866431-77-8
Molecular Formula:C₂₇H₃₇N₃O₆
Molecular Weight:499.607
Hs Code.:

Synonyms:isopropyl 3-amino-2-(4-tert-butyl-2-nitrophenoxy)-5-[(diisopropylamino)carbonyl]benzoate

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Chemical Property of isopropyl 3-amino-2-(4-tert-butyl-2-nitrophenoxy)-5-[(diisopropylamino)carbonyl]benzoate

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Technology Process of isopropyl 3-amino-2-(4-tert-butyl-2-nitrophenoxy)-5-[(diisopropylamino)carbonyl]benzoate

There total 5 articles about isopropyl 3-amino-2-(4-tert-butyl-2-nitrophenoxy)-5-[(diisopropylamino)carbonyl]benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 866431-76-7
isopropyl 2-(4-tert-butyl-2-nitrophenoxy)-5-[(diisopropylamino)carbonyl]-3-nitrobenzoate

: 866431-77-8
isopropyl 3-amino-2-(4-tert-butyl-2-nitrophenoxy)-5-[(diisopropylamino)carbonyl]benzoate

Guidance literature:: With iron; acetic acid; In methanol; dichloromethane; at 35 ℃; for 0.5h;
DOI:10.1002/hlca.200590133

Reference yield:

: 4-bromo-5-nitro-isophthaloyl dichloride

: 866431-77-8
isopropyl 3-amino-2-(4-tert-butyl-2-nitrophenoxy)-5-[(diisopropylamino)carbonyl]benzoate

Guidance literature:: Multi-step reaction with 3 steps

1: 112 g / Et₃N / CCl₄ / 0 °C

2: 90 percent / dimethylformamide / 2 h / 90 °C

3: 74 percent / Fe powder; AcOH / methanol; CH₂Cl₂ / 0.5 h / 35 °C

With iron; acetic acid; triethylamine; In methanol; tetrachloromethane; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1002/hlca.200590133

Reference yield:

: 866431-75-6
isopropyl 2-bromo-5-[(diisopropylamino)carbonyl]-3-nitrobenzoate

: 866431-77-8
isopropyl 3-amino-2-(4-tert-butyl-2-nitrophenoxy)-5-[(diisopropylamino)carbonyl]benzoate

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / dimethylformamide / 2 h / 90 °C

2: 74 percent / Fe powder; AcOH / methanol; CH₂Cl₂ / 0.5 h / 35 °C

With iron; acetic acid; In methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1002/hlca.200590133