isopropyl 2-(4-tert-butyl-2-nitrophenoxy)-5-[(diisopropylamino)carbonyl]-3-nitrobenzoate

Base Information

Chemical Name:isopropyl 2-(4-tert-butyl-2-nitrophenoxy)-5-[(diisopropylamino)carbonyl]-3-nitrobenzoate
CAS No.:866431-76-7
Molecular Formula:C₂₇H₃₅N₃O₈
Molecular Weight:529.59
Hs Code.:

Synonyms:isopropyl 2-(4-tert-butyl-2-nitrophenoxy)-5-[(diisopropylamino)carbonyl]-3-nitrobenzoate

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Chemical Property of isopropyl 2-(4-tert-butyl-2-nitrophenoxy)-5-[(diisopropylamino)carbonyl]-3-nitrobenzoate

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Technology Process of isopropyl 2-(4-tert-butyl-2-nitrophenoxy)-5-[(diisopropylamino)carbonyl]-3-nitrobenzoate

There total 4 articles about isopropyl 2-(4-tert-butyl-2-nitrophenoxy)-5-[(diisopropylamino)carbonyl]-3-nitrobenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 866431-75-6
isopropyl 2-bromo-5-[(diisopropylamino)carbonyl]-3-nitrobenzoate

: 4-t-butyl-2-nitrophenolate potassium salt

: 866431-76-7
isopropyl 2-(4-tert-butyl-2-nitrophenoxy)-5-[(diisopropylamino)carbonyl]-3-nitrobenzoate

Guidance literature:: In N,N-dimethyl-formamide; at 90 ℃; for 2h;
DOI:10.1002/hlca.200590133

Reference yield:

: 4-bromo-5-nitro-isophthaloyl dichloride

: 866431-76-7
isopropyl 2-(4-tert-butyl-2-nitrophenoxy)-5-[(diisopropylamino)carbonyl]-3-nitrobenzoate

Guidance literature:: Multi-step reaction with 2 steps

1: 112 g / Et₃N / CCl₄ / 0 °C

2: 90 percent / dimethylformamide / 2 h / 90 °C

With triethylamine; In tetrachloromethane; N,N-dimethyl-formamide;
DOI:10.1002/hlca.200590133

Reference yield:

: 6939-93-1
4-bromo-isophthalic acid

: 866431-76-7
isopropyl 2-(4-tert-butyl-2-nitrophenoxy)-5-[(diisopropylamino)carbonyl]-3-nitrobenzoate

Guidance literature:: Multi-step reaction with 4 steps

1: 84 percent / H₂SO₄; HNO₃ / H₂O / 0.5 h / 100 °C

2: PCl₅ / CH₂Cl₂ / cooling

3: 112 g / Et₃N / CCl₄ / 0 °C

4: 90 percent / dimethylformamide / 2 h / 90 °C

With phosphorus pentachloride; sulfuric acid; nitric acid; triethylamine; In tetrachloromethane; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1002/hlca.200590133