dotriacontane-1,32-diol

Base Information

Chemical Name:dotriacontane-1,32-diol
CAS No.:85756-62-3
Molecular Formula:C₃₂H₆₆O₂
Molecular Weight:482.875
Hs Code.:

Synonyms:dotriacontane-1,32-diol

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Chemical Property of dotriacontane-1,32-diol

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Technology Process of dotriacontane-1,32-diol

There total 17 articles about dotriacontane-1,32-diol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 670241-69-7
dotriaconta-1,31-diene

: 85756-62-3
dotriacontane-1,32-diol

Guidance literature:: dotriaconta-1,31-diene; With diisoamyl borane; In tetrahydrofuran; at 20 ℃;

With sodium hydroxide; dihydrogen peroxide; In tetrahydrofuran; ethanol; at 50 ℃; for 3h; Further stages.;
DOI:10.1002/chem.200601866

Reference yield: 92.0%

: 14606-66-7
dotriacontanedioic acid dimethyl ester

: 85756-62-3
dotriacontane-1,32-diol

Guidance literature:: With lithium aluminium tetrahydride; In tetrahydrofuran; at 0 - 90 ℃; for 3.25h; under 15001.5 Torr; Schlenk technique;
DOI:10.1002/anie.201702796

Reference yield:

: 59101-28-9
16-bromohexadecan-1-ol

: 85756-62-3
dotriacontane-1,32-diol

Guidance literature:: Multi-step reaction with 3 steps

1.1: pyridinium p-toluenesulfonate / CH₂Cl₂ / 24 h / 20 °C

2.1: magnesium / tetrahydrofuran / 3 h / 55 °C

2.2: dilithium tetrachlorocuprate(II) / tetrahydrofuran / 3 h / 0 °C

3.1: 5.8 g / pyridinium p-toluenesulfonate / methanol / 3 h / Heating

With pyridinium p-toluenesulfonate; magnesium; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.1002/chem.200601866