2,6-anhydro-3,4,5,7-tetra-O-benzyl-(1S)-C-phenyl-D-erythro-L-guloheptitol

Base Information

Chemical Name:2,6-anhydro-3,4,5,7-tetra-O-benzyl-(1S)-C-phenyl-D-erythro-L-guloheptitol
CAS No.:136034-22-5
Molecular Formula:C₄₁H₄₂O₆
Molecular Weight:630.781
Hs Code.:

Synonyms:2,6-anhydro-3,4,5,7-tetra-O-benzyl-(1S)-C-phenyl-D-erythro-L-guloheptitol

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Chemical Property of 2,6-anhydro-3,4,5,7-tetra-O-benzyl-(1S)-C-phenyl-D-erythro-L-guloheptitol

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Technology Process of 2,6-anhydro-3,4,5,7-tetra-O-benzyl-(1S)-C-phenyl-D-erythro-L-guloheptitol

There total 15 articles about 2,6-anhydro-3,4,5,7-tetra-O-benzyl-(1S)-C-phenyl-D-erythro-L-guloheptitol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 136034-19-0
(2S,4S,4aS,6R,7R,8S,8aR)-7,8-Bis-benzyloxy-6-benzyloxymethyl-2,4-diphenyl-hexahydro-pyrano[3,2-d][1,3]dioxine

: 136034-22-5
2,6-anhydro-3,4,5,7-tetra-O-benzyl-(1S)-C-phenyl-D-erythro-L-guloheptitol

Guidance literature:: With lithium aluminium tetrahydride; aluminium trichloride;

Reference yield: 66.0%

: phenylmagnesium bromide

: 113019-43-5,140397-45-1,140397-46-2,140397-47-3,140397-49-5,91738-17-9
2,3,4,6-tetra-O-benzyl-1-formyl-D-glucopyranose

: 136034-22-5
(R)-Phenyl-((2S,3R,4S,5R,6R)-3,4,5-tris-benzyloxy-6-benzyloxymethyl-tetrahydro-pyran-2-yl)-methanol

Guidance literature:: In tetrahydrofuran; at -78 ℃; for 3.5h;
DOI:10.1039/b705750d

Reference yield: 17.0%

: 216869-51-1
(1(1')-Z)-2,3,4,6-tetra-O-benzyl-1-deoxy-1-(phenyl)methylidene-D-glucopyranose

: 136034-22-5
2,6-anhydro-3,4,5,7-tetra-O-benzyl-(1S)-C-phenyl-D-erythro-L-guloheptitol

: 2,6-anhydro-3,4,5,7-tetra-O-benzyl-1-C-phenyl-D-erythro-L-guloheptitol

Guidance literature:: (1(1')-Z)-2,3,4,6-tetra-O-benzyl-1-deoxy-1-(phenyl)methylidene-D-glucopyranose; With borane; In tetrahydrofuran; for 72h;

With sodium hydroxide; dihydrogen peroxide; at 20 ℃; for 0.5h;
DOI:10.1002/1099-0690(200204)2002:7<1323::AID-EJOC1323>3.0.CO;2-8