dimethyl 6-chlorofuro[3,2-b]pyridine-2,3-dicarboxylate

Base Information

• Chemical Name: dimethyl 6-chlorofuro[3,2-b]pyridine-2,3-dicarboxylate
• CAS No.: 56159-18-3
• Molecular Formula: C₁₁H₈ClNO₅
• Molecular Weight: 269.641
• Mol file: 56159-18-3.mol

Synonyms:Furo[3,2-b]pyridine-2,3-dicarboxylicacid, 6-chloro-, dimethyl ester (9CI); NSC 242975

Chemical Property of dimethyl 6-chlorofuro[3,2-b]pyridine-2,3-dicarboxylate

Chemical Property:

• Vapor Pressure: 0.000147mmHg at 25°C
• Boiling Point: 332.3°Cat760mmHg
• Flash Point: 154.8°C
• Density: 1.439g/cm³

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of dimethyl 6-chlorofuro[3,2-b]pyridine-2,3-dicarboxylate

There total 2 articles about dimethyl 6-chlorofuro[3,2-b]pyridine-2,3-dicarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3,5-dicholoropyridine N-oxide (15177-57-8) + dimethyl acetylenedicarboxylate (762-42-5) → 7-chloro-furo[3,2-c]pyridine-2,3-dicarboxylic acid dimethyl ester (56159-19-4) + 6-chloro-furo[3,2-b]pyridine-2,3-dicarboxylic acid dimethyl ester (56159-18-3)

Guidance literature:

In toluene;

DOI:10.1021/ja00844a057

Reference yield:

3,5-dicholoropyridine N-oxide (15177-57-8) + dimethyl acetylenedicarboxylate (762-42-5) → 6-chloro-furo[3,2-b]pyridine-2,3-dicarboxylic acid dimethyl ester (56159-18-3)

Guidance literature:

In toluene;

DOI:10.1021/ja00844a057

upstream raw materials:

3,5-dicholoropyridine N-oxide

dimethyl acetylenedicarboxylate